6-methoxy-3-phenyl-1-tetralin

Base Information

Chemical Name:6-methoxy-3-phenyl-1-tetralin
CAS No.:93273-56-4
Molecular Formula:C₂₉H₃₃NO₂
Molecular Weight:427.587
Hs Code.:

6-methoxy-3-phenyl-1-<p-(β-pyrrolidinoethoxy)-phenyl>tetralin

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methoxy-3-phenyl-1-tetralin

Chemical Property:

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Technology Process of 6-methoxy-3-phenyl-1-tetralin

There total 10 articles about 6-methoxy-3-phenyl-1-tetralin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 7250-67-1
1-(2-chloroethyl)pyrrolidine hydrochloride

: 93300-82-4
1-(p-hydroxyphenyl)-6-methoxy-3-phenyltetralin

: 93273-56-4
6-methoxy-3-phenyl-1-tetralin

Guidance literature:: With potassium carbonate; In acetone; for 12h; Heating;

Reference yield:

: 93300-81-3
β-(m-methoxyphenyl)-α-phenylpropionic acid

: 93273-56-4
6-methoxy-3-phenyl-1-tetralin

Guidance literature:: Multi-step reaction with 10 steps

1: 95 percent / H₂SO₄ / 12 h / Heating

2: 66 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

3: 70 percent / pyridine / 12 h / Ambient temperature

4: 76 percent / dimethylformamide / 12 h / Ambient temperature

5: 79 percent / 2N NaOH / ethane-1,2-diol / 18 h / Heating

6: PCl₅ / benzene / 1 h / Heating

7: SnCl₄ / benzene / 6 h / Ambient temperature

8: 95 percent / KBH₄ / methanol / 3 h / Ambient temperature

9: 50 percent / AlCl₃ / benzene; hexane / 30 h / Ambient temperature

10: 82 percent / K₂CO₃ / acetone / 12 h / Heating

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; potassium borohydride; phosphorus pentachloride; sulfuric acid; tin(IV) chloride; potassium carbonate; In methanol; diethyl ether; hexane; ethylene glycol; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 93273-51-9
3-(m-methoxyphenyl)-2-phenylpropan-1-ol

: 93273-56-4
6-methoxy-3-phenyl-1-tetralin

Guidance literature:: Multi-step reaction with 8 steps

1: 70 percent / pyridine / 12 h / Ambient temperature

2: 76 percent / dimethylformamide / 12 h / Ambient temperature

3: 79 percent / 2N NaOH / ethane-1,2-diol / 18 h / Heating

4: PCl₅ / benzene / 1 h / Heating

5: SnCl₄ / benzene / 6 h / Ambient temperature

6: 95 percent / KBH₄ / methanol / 3 h / Ambient temperature

7: 50 percent / AlCl₃ / benzene; hexane / 30 h / Ambient temperature

8: 82 percent / K₂CO₃ / acetone / 12 h / Heating

With pyridine; sodium hydroxide; aluminium trichloride; potassium borohydride; phosphorus pentachloride; tin(IV) chloride; potassium carbonate; In methanol; hexane; ethylene glycol; N,N-dimethyl-formamide; acetone; benzene;