Technology Process of 2,4,6-Tri-tert-butylbenzenesulfenyl bromide
There total 3 articles about 2,4,6-Tri-tert-butylbenzenesulfenyl bromide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
bromine;
In
tetrachloromethane;
Ambient temperature;
DOI:10.1021/jo00056a026
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3.0 g / K3, 10percent NaOH / diethyl ether
2: Br2 / CCl4 / Ambient temperature
With
sodium hydroxide; bromine; potassium hexacyanoferrate(III);
In
tetrachloromethane; diethyl ether;
DOI:10.1021/jo00056a026
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) S, 2.) LiAlH4 / 1.a) THF, -20 deg C up to rt, b) rt, overnight, 2.) reflux, 1 h
2: 3.0 g / K3, 10percent NaOH / diethyl ether
3: Br2 / CCl4 / Ambient temperature
With
sodium hydroxide; lithium aluminium tetrahydride; bromine; potassium hexacyanoferrate(III);
In
tetrachloromethane; diethyl ether;
DOI:10.1021/jo00056a026
