(3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

Base Information

Chemical Name:(3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide
CAS No.:1309251-02-2
Molecular Formula:C₄₃H₈₁N₅O₈
Molecular Weight:796.145
Hs Code.:

(3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

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Chemical Property of (3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

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Technology Process of (3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

There total 14 articles about (3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: C₁₉H₃₆N₂O₅

: 1309251-01-1
C₂₄H₄₇N₃O₄*ClH

: 1309251-02-2
(3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide;

Reference yield:

: 67010-43-9
(3S,4S)-ethyl 4-(tert-butoxycarbonylamino)-3-hydroxy-6-methylheptanoate

: 1309251-02-2
(3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

Guidance literature:: Multi-step reaction with 6 steps

1: water / Alkaline conditions

2: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 1.5 h / -15 - 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

4: benzotriazol-1-ol; dicyclohexyl-carbodiimide

5: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

6: benzotriazol-1-ol; dicyclohexyl-carbodiimide

With 4-methyl-morpholine; hydrogenchloride; water; benzotriazol-1-ol; dicyclohexyl-carbodiimide; isobutyl chloroformate; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 103808-88-4
C₁₈H₃₆N₂O₄

: 1309251-02-2
(3S,4S)-4-((3S,4S)-4-((3S,4S)-4-(ε-(N-isovalerylamino)hexanoyl)amino-3-hydroxy-6-methylheptanoylamino)-5-cyclohexyl-3-hydroxypentanoylamino)-3-hydroxy-6-methylheptanoic acid N-isoamylamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

2: benzotriazol-1-ol; dicyclohexyl-carbodiimide

3: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

4: benzotriazol-1-ol; dicyclohexyl-carbodiimide

With hydrogenchloride; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane;