5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol

Base Information

Chemical Name:5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol
CAS No.:1027306-62-2
Molecular Formula:C₁₀H₁₆S
Molecular Weight:168.303
Hs Code.:

Synonyms:

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Chemical Property of 5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol

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Technology Process of 5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol

There total 2 articles about 5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 155996-11-5
5,5-dimethy-3-vinyl-2-cyclohexenyl thioacetate

: 1027306-62-2
5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol

Guidance literature:: With potassium hydroxide; In ethanol; for 0.166667h; Ambient temperature;
DOI:10.1021/jo00086a010

Reference yield:

: 84132-65-0
rac-5,5-dimethyl-3-vinylcyclohex-2-en-1-ol

: 1027306-62-2
5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / N,N-dimethylformamide dineopentyl acetal / toluene / 0.17 h / 0 °C

2: 0.2 N KOH / ethanol / 0.17 h / Ambient temperature

With potassium hydroxide; N,N-dimethylformamide dineopentyl acetal; In ethanol; toluene;
DOI:10.1021/jo00086a010

Reference yield:

: 1027306-62-2
5,5-Dimethyl-3-vinyl-cyclohex-2-enethiol

: 155996-25-1
5,5-dimethyl-1-(2-propynylsulfonyl)-3-vinyl-2-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: Bu₄NHSO₄, 6percent aq. NaOH / benzene / 0.5 h / Ambient temperature

2: 91 percent / 80percent m-CPBA / CH₂Cl₂ / 0.33 h / 0 °C

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1021/jo00086a010