Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine

Base Information

• Chemical Name: Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine
• CAS No.: 96802-12-9
• Molecular Formula: C₆H₁₅N*C₃₃H₂₇ClN₅O₇P
• Molecular Weight: 773.225

Synonyms:

Chemical Property of Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine

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Technology Process of Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine

There total 3 articles about Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

triethylamine carbonate (15715-58-9) + 9-(hydroxyethoxymethyl)-2-N-(9-phenylxanthen-9-yl)-guanine (96802-10-7) → Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine (96802-12-9)

Guidance literature:

In pyridine;

DOI:10.3891/acta.chem.scand.39b-0047

Reference yield:

acycloguanosine (59277-89-3) → Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine (96802-12-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 95 percent / pyridine

In pyridine;

DOI:10.3891/acta.chem.scand.39b-0047

Reference yield:

pixyl chloride (42506-03-6) → Phosphoric acid 2-chloro-phenyl ester 2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethyl ester; compound with triethyl-amine (96802-12-9)

Guidance literature:

Multi-step reaction with 2 steps

2: 95 percent / pyridine

In pyridine;

DOI:10.3891/acta.chem.scand.39b-0047

upstream raw materials:

triethylamine carbonate

9-(hydroxyethoxymethyl)-2-N-(9-phenylxanthen-9-yl)-guanine

acycloguanosine

pixyl chloride

Downstream raw materials:

Tetradecanoic acid 2-((2-chloro-phenoxy)-{2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethoxy}-phosphoryloxy)-1-tetradecanoyloxymethyl-ethyl ester

Tetradecanoic acid 2-(hydroxy-{2-[6-oxo-2-(9-phenyl-9H-xanthen-9-ylamino)-1,6-dihydro-purin-9-ylmethoxy]-ethoxy}-phosphoryloxy)-1-tetradecanoyloxymethyl-ethyl ester; compound with triethyl-amine

Tetradecanoic acid 2-[[2-(2-amino-6-oxo-1,6-dihydro-purin-9-ylmethoxy)-ethoxy]-(2-chloro-phenoxy)-phosphoryloxy]-1-tetradecanoyloxymethyl-ethyl ester

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