Ph₃GeGe(Bu)2H

Base Information

Chemical Name:Ph₃GeGe(Bu)2H
CAS No.:894804-43-4
Molecular Formula:C₂₆H₃₄Ge₂
Molecular Weight:491.736
Hs Code.:

Synonyms:

Suppliers and Price of Ph₃GeGe(Bu)2H

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ph₃GeGe(Bu)2H

Chemical Property:

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Technology Process of Ph₃GeGe(Bu)2H

There total 1 articles about Ph₃GeGe(Bu)2H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 894804-40-1
Ph₃GeGeBu(n)2CH₂CH₂OEt

: 102854-88-6
diisobutylaluminium hydride

: 894804-43-4
Ph₃GeGe(Bu)2H

Guidance literature:: In hexane; benzene; byproducts: i-Bu2AlOEt, H2CCH2; under inert atm. to soln. Ph3GeGe(Bu)2CH2CH2OEt in benzene soln. DIBAL-Hin hexane was added and refluxed for 18 h; volatiles were removed in vacuo, residue was filtered through silica column (hexane), solvent was removed in vacuo; elem. anal.;
DOI:10.1021/om060115x

Reference yield: 94.0%

: 894804-36-5
Bu₂Ge(NMe₂)CH₂CH₂OEt

: 894804-43-4
Ph₃GeGe(Bu)2H

: 894804-44-5
Ph₃GeGeBu(n)2GeBu(n)2CH₂CH₂OEt

Guidance literature:: In acetonitrile; High Pressure; under inert atm. to soln. Ph3GeGe(Bu)2H in MeCN soln. Bu2Ge(NMe2)CH2CH2OEt in MeCN was added and heated in tube sealed with Teflon plug at 85°C for 48 h; volatiles were removed in vacuo, residue was distilled in Kugelrohr oven(100°C, 0.08 Torr) for 3 h; elem. anal.;
DOI:10.1021/om060115x

Reference yield:

: 894804-43-4
Ph₃GeGe(Bu)2H

: 894804-46-7
Ph₃GeGe(Bu)2Ge(Bu)2Ge(Bu)2CH₂CH₂OEt

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile

2: benzene; hexane

3: acetonitrile

In hexane; acetonitrile; benzene;
DOI:10.1021/om060115x