[(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol

Base Information

Chemical Name:[(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol
CAS No.:2345-68-8
Molecular Formula:C₅H₁₀O₂
Molecular Weight:102.133
Hs Code.:
DSSTox Substance ID:DTXSID001283388
Nikkaji Number:J1.185.203C

Synonyms:[(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol;2345-68-8;[(1R,2S)-2-(hydroxymethyl)cyclopropyl]methanol;rel-(1R,2S)-Cyclopropane-1,2-diyldimethanol;SCHEMBL5052791;DTXSID001283388;cis-cyclopropane-1,2-diyldimethanol;MFCD30218954;Cyclopropane-1alpha,2alpha-dimethanol;AS-53426;rel-(1R,2S)-1,2-Cyclopropanedimethanol;1,2-Cyclopropanedimethanol, (1R,2S)-rel-;cis-2-(Hydroxymethyl)cyclopropyl-1-methanol;CS-0053077;P16470;EN300-7369839;192056-11-4

Suppliers and Price of [(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 8 raw suppliers

Chemical Property of [(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol

Chemical Property:

XLogP3:-0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:102.068079557
Heavy Atom Count:7
Complexity:55.1

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C(C1CO)CO
Isomeric SMILES:C1[C@@H]([C@@H]1CO)CO

Technology Process of [(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol

There total 1 articles about [(1S,2R)-rel-2-(hydroxymethyl)cyclopropyl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 826-34-6
dimethyl cis-cyclopropane-1,2-dicarboxylate

: 2345-68-8,192056-11-4
((1R,2S)-2-Hydroxymethyl-cyclopropyl)-methanol

Guidance literature:: With lithium aluminium tetrahydride;
DOI:10.1016/S0040-4039(00)94782-8 DOI:10.1021/ja00381a024

Reference yield: 97.0%

: 2345-68-8,192056-11-4
((1R,2S)-2-Hydroxymethyl-cyclopropyl)-methanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: cis-2-(tert-butyldiphenylsilyloxymethyl)cyclopropylmethanol

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0960-894X(97)00420-4

Reference yield: 49.5%

: 17739-45-6,59146-56-4
2-(2-bromoethoxy)tetrahydropyran

: 2345-68-8,192056-11-4
((1R,2S)-2-Hydroxymethyl-cyclopropyl)-methanol

: rac-((1R,2S)-2-((2-((tetrahydro-2H-pyran-2-yl)oxy)ethoxy)methyl)cyclopropyl)methanol

Guidance literature:: ((1R,2S)-2-Hydroxymethyl-cyclopropyl)-methanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.75h; Inert atmosphere;

2-(2-bromoethoxy)tetrahydropyran; In tetrahydrofuran; mineral oil; at 20 - 65 ℃; for 120h; Inert atmosphere;