(2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α⁵α⁵,α^5'''',α^5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol

Base Information

• Chemical Name: (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α⁵α⁵,α^5'''',α^5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol
• CAS No.: 494198-66-2
• Molecular Formula: C₃₀H₅₂O₇
• Molecular Weight: 524.739

Synonyms:

Chemical Property of (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α⁵α⁵,α^5'''',α^5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol

Chemical Property:

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Safty Information:

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Useful:

Technology Process of (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α⁵α⁵,α^5'''',α^5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol

There total 2 articles about (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α⁵α⁵,α^5'''',α^5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

(α5RS,2RS,2'SR,2''SR,2'''SR,5SR,5'RS,5''RS,5'''RS)-hexadecahydro-α5α5''',α5''',2,2'',2'''-hexamethyl-α5-(4-methylpent-3-en-1-yl)-[2,2':5',2'':5'',2'''-quaterfuran]-55'''-dimethanol → (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''RS)-eicosahydrooctamethyl-α5α5,α5'''',α5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol (494198-66-2,172670-58-5) + (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α5α5,α5'''',α5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol (494198-66-2,172670-58-5)

Guidance literature:

With disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1002/hlca.200890137

Reference yield: 41.0%

(α5RS,2RS,2'SR,2''SR,2'''SR,5SR,5'RS,5''RS,5'''RS)-hexadecahydro-α5α5''',α5''',2,2'',2'''-hexamethyl-α5-(4-methylpent-3-en-1-yl)-[2,2':5',2'':5'',2'''-quaterfuran]-55'''-dimethanol → (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''RS)-eicosahydrooctamethyl-α5α5,α5'''',α5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol (494198-66-2,172670-58-5) + (2RS,2'SR,2''SR,2'''SR,2''''SR,5SR,5'RS,5''RS,5'''RS,5''''SR)-eicosahydrooctamethyl-α5α5,α5'''',α5''''2,2''',2'''',5'-[2,2':5',2'':5'',2''';5''',2''''-quinquefuran]-5,5'''''-dimethanol (494198-66-2,172670-58-5)

Guidance literature:

With disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 3h;

DOI:10.1002/hlca.200890137

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