[Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)]

Base Information

Chemical Name:[Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)]
CAS No.:93122-14-6
Molecular Formula:C₂₄H₁₇CrNO₄S₂
Molecular Weight:499.531
Hs Code.:

[Cr(CNC<sub>6</sub>H<sub>5</sub>)(CO)4(S(C<sub>6</sub>H<sub>5</sub>)CH<sub>2</sub>SC<sub>6</sub>H<sub>5</sub>)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)]

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Technology Process of [Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)]

There total 1 articles about [Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 505-23-7
1,3 dithiane

: 14782-94-6
pentacarbonyl(phenylisocyanide)chromium

: 93122-14-6
[Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)]

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); a stirred soln. of complex and dithiane in THF was irradiated with UV light for 4 h; solvent was removed in vac., residue was chromd.; elem.anal.;

Reference yield: 24.0%

: 1748-15-8
1,3-dithiane-2-thione

: 93122-14-6
[Cr(CNC₆H₅)(CO)4(S(C₆H₅)CH₂SC₆H₅)]

: 368-39-8
triethyloxonium fluoroborate

: 93122-20-4
[Cr(CNC₆H₅)(CO)4(SCS(CH₂)2S)]

Guidance literature:: With n-butyllithium; In tetrahydrofuran; to a stirred soln. of complex in THF at -60°C was added LiBu, after 5 min SCS(CH2)3S was added dropwise, the mixt. was stirred for 1 h at -60°C and then the mixt. was allowed to attain room temp.; solvent was evapd., residue was dissolved in CH2Cl2, (Et3O)BF4 was added and mixt. was filtered through SiO2, the solvent was removed and residue was chromd., ppt. was recrystd. twice from hexane/Et2O (-30°C); elem.anal.;