(N(Me₃SiNCH₂CH₂)3)ZrNH=NCPh₂

Base Information

• Chemical Name: (N(Me₃SiNCH₂CH₂)3)ZrNH=NCPh₂
• CAS No.: 1093406-82-6
• Molecular Formula: C₂₈H₅₀N₆Si₃Zr
• Molecular Weight: 646.226
• Mol file: 1093406-82-6.mol

Synonyms:

Chemical Property of (N(Me₃SiNCH₂CH₂)3)ZrNH=NCPh₂

Chemical Property:

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Technology Process of (N(Me₃SiNCH₂CH₂)3)ZrNH=NCPh₂

There total 1 articles about (N(Me₃SiNCH₂CH₂)3)ZrNH=NCPh₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

([κ5-N,N,N,N,C-(Me3SiNCH2CH2)2NCH2CH2NSiMe2CH2]Zr + benzophenone hydrazone (5350-57-2) → (N(Me3SiNCH2CH2)3)ZrNH=NCPh2 (1093406-82-6)

Guidance literature:

In diethyl ether; (N2); mixture of zirconium complex, benzophenone hydrazone and Et2O was stirred for 30 min at ambient temp.; crystd. at -30°C, elem. anal.;

DOI:10.1021/om8008684

upstream raw materials:

benzophenone hydrazone