26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.0^7,12]octacosa-1⁽²⁷⁾,7,9,11,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

Base Information

• Chemical Name: 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.0^7,12]octacosa-1⁽²⁷⁾,7,9,11,24⁽²⁸⁾,25-hexaene-28-carboxylic acid
• CAS No.: 124199-83-3
• Molecular Formula: C₃₈H₅₀O₉
• Molecular Weight: 650.81

Synonyms:

Chemical Property of 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.0^7,12]octacosa-1⁽²⁷⁾,7,9,11,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.0^7,12]octacosa-1⁽²⁷⁾,7,9,11,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

There total 7 articles about 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.0^7,12]octacosa-1⁽²⁷⁾,7,9,11,24⁽²⁸⁾,25-hexaene-28-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.07,12]octacosa-1(27),7,9,11,24(28),25-hexaene-28-carboxylic acid methyl ester → 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.07,12]octacosa-1(27),7,9,11,24(28),25-hexaene-28-carboxylic acid (124199-83-3)

Guidance literature:

With potassium hydroxide; In ethanol; for 18h; Heating;

DOI:10.1021/jm00164a048

Reference yield:

1-hydroxy-2-<2-<2-(2-hydroxyethoxy)ethoxy>ethoxy>benzene (65659-36-1) → 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.07,12]octacosa-1(27),7,9,11,24(28),25-hexaene-28-carboxylic acid (124199-83-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 73 percent / diisopropylethylamine / 18 h / 125 °C

2: 55 percent / 50percent sodium hydride / tetrahydrofuran / Ambient temperature

3: 1.4 M KOH / ethanol / 18 h / Heating

With potassium hydroxide; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol;

DOI:10.1021/jm00164a048

Reference yield:

2-(2'-(2''-Chloroethoxy)ethoxy)ethyl-2-tetrahydro-2H-pyran (85539-28-2) → 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.07,12]octacosa-1(27),7,9,11,24(28),25-hexaene-28-carboxylic acid (124199-83-3)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium carbonate / dimethylformamide / 18 h / 140 °C

2: 1 N HCl / methanol / Ambient temperature

3: 73 percent / diisopropylethylamine / 18 h / 125 °C

4: 55 percent / 50percent sodium hydride / tetrahydrofuran / Ambient temperature

5: 1.4 M KOH / ethanol / 18 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00164a048

upstream raw materials:

1-hydroxy-2-<2-<2-(2-hydroxyethoxy)ethoxy>ethoxy>benzene

2-(2'-(2''-Chloroethoxy)ethoxy)ethyl-2-tetrahydro-2H-pyran

methyl 2,6-bis(bromomethyl)-4-tert-butylbenzoate

2-(2-{2-[2-(Tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-phenol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 124199-83-3 26-tert-Butyl-4-(4-tert-butyl-phenoxymethyl)-3,6,13,16,19,22-hexaoxa-tricyclo[22.3.1.0^7,12]octacosa-1⁽²⁷⁾,7,9,11,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

Send

Send

Metric Ton KG G Pound L ML

Send

Send