C₂₆H₃₃BrN₆O₂S

Base Information

Chemical Name:C₂₆H₃₃BrN₆O₂S
CAS No.:958022-30-5
Molecular Formula:C₂₆H₃₃BrN₆O₂S
Molecular Weight:573.557
Hs Code.:

C<sub>26</sub>H<sub>33</sub>BrN<sub>6</sub>O<sub>2</sub>S

Synonyms:

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Chemical Property of C₂₆H₃₃BrN₆O₂S

Chemical Property:

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Technology Process of C₂₆H₃₃BrN₆O₂S

There total 6 articles about C₂₆H₃₃BrN₆O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852030-25-2
8-(7-bromo-2,3-dihydro-benzo[1,4]dioxin-6-ylsulfanyl)adenine

: 1396789-85-7
C₁₅H₂₉NO₃S

: 958022-30-5
C₂₆H₃₃BrN₆O₂S

Guidance literature:: With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; In N,N-dimethyl-formamide; at 80 ℃; for 10h;
DOI:10.1021/jm3004619

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 958022-30-5
C₂₆H₃₃BrN₆O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tris(acetoxy)borohydride / dichloromethane

2: base (NEt₃ or DMAP) / dichloromethane / 20 °C

3: N,N,N′,N′-tetramethyl-N″-tert-butylguanidine / N,N-dimethyl-formamide / 10 h / 80 °C

With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; sodium tris(acetoxy)borohydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm3004619

Reference yield:

: 7390-62-7
8-mercaptoadenine

: 958022-30-5
C₂₆H₃₃BrN₆O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane / 16 h / 100 °C / Inert atmosphere

2: N,N,N′,N′-tetramethyl-N″-tert-butylguanidine / N,N-dimethyl-formamide / 10 h / 80 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; potassium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/jm3004619