carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

Base Information

Chemical Name:carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine
CAS No.:135902-12-4
Molecular Formula:C₃₃H₃₉N₇O₁₀
Molecular Weight:693.714
Hs Code.:

<N<<N-(tert-butoxycarbonyl)-cis-4-aminocyclohexyl>carbonyl>phenylalanyl>-N<sup>im</sup>-(2,4-dinitrophenyl)histidine

Synonyms:

Suppliers and Price of carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

There total 2 articles about carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25024-53-7
Boc-His(Dnp)-OH

: 135902-12-4
carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

Guidance literature:: Multi-step reaction with 2 steps

1: 5.5M HCl / 1,2-dimethoxy-ethane / 5 h / Ambient temperature

2: NaHCO₃ / tetrahydrofuran; H₂O / 24 h / Ambient temperature

With hydrogenchloride; sodium hydrogencarbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water;
DOI:10.1021/jm00081a019

Reference yield:

: (S)-2-[(4-tert-Butoxycarbonylamino-cyclohexanecarbonyl)-amino]-3-phenyl-propionic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 25030-55-1
1-(2,4-dinitro-phenyl)-histidine

: 135902-12-4
carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; water; for 24h; Yield given; Ambient temperature;
DOI:10.1021/jm00081a019

Reference yield:

: 135902-12-4
carbonyl>phenylalanyl>-N^im-(2,4-dinitrophenyl)histidine

: 135901-93-8,138606-66-3
phenylalanyl>histydyl <(2S,3R,4R,5R,6R)-1-cyclohexyl-3,4,5,6,7-pentahydroxyhept-2-yl>amide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) pyvaloyl chloride, N-ethylpiperidine, Et₃N / 1.) CH₂Cl₂, RT, 10 min, 2.) CH₂Cl₂, RT, 20 h

2: thiophenol / acetonitrile / 2 h / Ambient temperature

3: 24 percent / trifluoroacetic acid / CH₂Cl₂ / 7 h / 0 °C / 15

With 1-ethyl-piperidine; pivaloyl chloride; thiophenol; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jm00081a019