2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride

Base Information

Chemical Name:2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride
CAS No.:29183-12-8
Molecular Formula:C₂₁H₂₁N₂O*Cl
Molecular Weight:352.864
Hs Code.:

2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benz<de>isoquinolinium chloride

Synonyms:

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Chemical Property of 2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride

Chemical Property:

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Technology Process of 2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride

There total 4 articles about 2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₂₀N₂O

: 29183-12-8
2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride

Guidance literature:: With hydrogenchloride; In ethanol; Yield given;
DOI:10.1039/P19810001154

Reference yield:

: 19961-48-9
2-Methyl-1,3-dihydrobenzisoquinoline

: 29183-12-8
2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / acetonitrile

2: 82 percent / aq. sodium hydroxide / 0 °C

3: CHCl₃ / 4 h / 0 - 5 °C

4: dry hydrogen chloride gas / ethanol

With hydrogenchloride; sodium hydroxide; In ethanol; chloroform; acetonitrile;
DOI:10.1039/P19810001154

Reference yield:

: 29183-40-2
anhydro<2-methyl-2-phenacyl-2,3-dihydro-1H-benzisoquinolinium hydroxide>

: 29183-12-8
2-methyl-2(N-phenylcarbamoylmethyl)-2,3-dihydro-1H-benzisoquinolinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 4 h / 0 - 5 °C

2: dry hydrogen chloride gas / ethanol

With hydrogenchloride; In ethanol; chloroform;
DOI:10.1039/P19810001154