2,4'-dimethoxy-4-nitrodiphenyl ether

Base Information

Chemical Name:2,4'-dimethoxy-4-nitrodiphenyl ether
CAS No.:77896-31-2
Molecular Formula:C₁₄H₁₃NO₅
Molecular Weight:275.261
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4'-dimethoxy-4-nitrodiphenyl ether

Chemical Property:

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Technology Process of 2,4'-dimethoxy-4-nitrodiphenyl ether

There total 2 articles about 2,4'-dimethoxy-4-nitrodiphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77337-82-7
1-bromo-2-methoxy-4-nitrobenzene

: 150-76-5
4-methoxy-phenol

: 77896-31-2
2,4'-dimethoxy-4-nitrodiphenyl ether

Guidance literature:: With copper; potassium carbonate; In pyridine; at 170 ℃; for 2h;
DOI:10.1039/P19810000493

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 77896-17-4
4-nitro-1,3-benzodioxole-2-spirocyclohexadien-4'-one

: 14064-92-7
2,4'-dimethoxy-5-nitrodiphenyl ether

: 77896-31-2
2,4'-dimethoxy-4-nitrodiphenyl ether

Guidance literature:: With sodium tetrahydroborate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) methanol, water;
DOI:10.1039/P19810000493

Reference yield:

: 77896-31-2
2,4'-dimethoxy-4-nitrodiphenyl ether

: 77896-08-3
2,4'-dihydroxy-5-nitrodiphenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine hydrochloride / 190 °C

2: 39 percent / active manganese dioxide / benzene / Heating

3: sodium borohydride / methanol; H₂O

With manganese(IV) oxide; sodium tetrahydroborate; pyridine hydrochloride; In methanol; water; benzene;
DOI:10.1039/P19810000493