2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester
CAS No.:1054667-20-7
Molecular Formula:C₂₅H₂₇Cl₃F₃NO₇S₂
Molecular Weight:680.978
Hs Code.:

2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of 2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of 2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester

There total 2 articles about 2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 358-23-6
trifluoromethylsulfonic anhydride

: 1055029-76-9
2,2,2-Trichloro-acetimidic acid (2R,3R,4S,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

: 1054667-20-7
2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.0833333h;
DOI:10.1039/b309823k

Reference yield:

: 152964-70-0
ethyl 2,3-di-O-benzyl-1-thio-β-D-glucopyranoside

: 1054667-20-7
2,2,2-Trichloro-acetimidic acid (2R,3R,4R,5R,6S)-4,5-bis-benzyloxy-6-ethylsulfanyl-3-trifluoromethanesulfonyloxy-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 0.75 h / 0 °C

2: pyridine / CH₂Cl₂ / 0.08 h / 0 °C

With pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1039/b309823k