Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

Base Information

Chemical Name:Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide
CAS No.:164988-80-1
Molecular Formula:C₇₀H₁₀₅NO₈
Molecular Weight:1088.61
Hs Code.:

Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

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Technology Process of Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

There total 3 articles about Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-78-4
(2S,3R,4E)-2-amino-4-octadecene-1,3-diol

: 164988-80-1
Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine / tetrahydrofuran / 12 h / 40 °C

2: 1.) SnCl₂, AgClO₄, 4 Angstroem sieves / 1.) THF, RT, 30 min, 2.) THF, from -10 deg C to RT, 2 h

With dmap; 4 A molecular sieve; silver perchlorate; tin(ll) chloride; In tetrahydrofuran;
DOI:10.1021/jm00012a018

Reference yield:

: 14617-86-8
4-nitrophenyl stearate

: 164988-80-1
Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 4-(dimethylamino)pyridine / tetrahydrofuran / 12 h / 40 °C

2: 1.) SnCl₂, AgClO₄, 4 Angstroem sieves / 1.) THF, RT, 30 min, 2.) THF, from -10 deg C to RT, 2 h

With dmap; 4 A molecular sieve; silver perchlorate; tin(ll) chloride; In tetrahydrofuran;
DOI:10.1021/jm00012a018

Reference yield:

: 54336-64-0,95037-06-2,104826-38-2,123482-90-6,134731-78-5,136846-30-5,2304-81-6,252039-52-4
(2S,3R,4E)-2-(N-stearoylamino)-4-octadecene-1,3-diol

: 143615-35-4
2,3,4,6-tetra-O-benzyl-D-galactopyranosyl fluoride

: 164988-80-1
Octadecanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide

Guidance literature:: With 4 A molecular sieve; silver perchlorate; tin(ll) chloride; Multistep reaction; 1.) THF, RT, 30 min, 2.) THF, from -10 deg C to RT, 2 h;
DOI:10.1021/jm00012a018