N-[(2-methylphenyl)phenylsulfonio]-N-[(4-methylbenzene)dioxosulfanyl]aminylene

Base Information

• Chemical Name: N-[(2-methylphenyl)phenylsulfonio]-N-[(4-methylbenzene)dioxosulfanyl]aminylene
• CAS No.: 53897-89-5
• Molecular Formula: C₂₀H₁₉NO₂S₂
• Molecular Weight: 369.508
• Mol file: 53897-89-5.mol

Synonyms:

Chemical Property of N-[(2-methylphenyl)phenylsulfonio]-N-[(4-methylbenzene)dioxosulfanyl]aminylene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-[(2-methylphenyl)phenylsulfonio]-N-[(4-methylbenzene)dioxosulfanyl]aminylene

There total 2 articles about N-[(2-methylphenyl)phenylsulfonio]-N-[(4-methylbenzene)dioxosulfanyl]aminylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(phenylthio)toluene (13963-35-4) + sodium p-toluenesulfonamide (18522-92-4) → S-(o-methylphenyl)-S-phenyl-N-tosylsulfilimine (53897-89-5,59345-35-6)

Guidance literature:

With pyridine; tert-butylhypochlorite; (-)-menthol; Mechanism; multistep reaction, enantioselectivity study;

DOI:10.1246/bcsj.58.1934

Reference yield:

→ S-(o-methylphenyl)-S-phenyl-N-tosylsulfilimine (53897-89-5,59345-35-6)

Guidance literature:

entspr. Sulfid, (-)-Menthol, (CH3)3COCl, /BRN= 576241/;

Reference yield:

S-(o-methylphenyl)-S-phenyl-N-tosylsulfilimine (53897-89-5,59345-35-6) → o-Methyldiphenylsulphilimin

Guidance literature:

With sulfuric acid;

DOI:10.1016/0040-4020(76)80159-7

upstream raw materials:

2-(phenylthio)toluene

sodium p-toluenesulfonamide

Downstream raw materials:

o-Methyldiphenylsulphilimin