NH₂(CH₂C₆H₄C(CH₃)3)2⁽¹⁺⁾*PF₆^(1-)*[Ni((C₆H₄NCHC₆H₃(O)O(C₂H₄O)2)2)]=[Ni(C₆H₄NCHC₆H₃O₂(C₂H₄O)2)2]H₂N(CH₂C₆H₄C(CH₃)3)2PF₆

Base Information

• Chemical Name: NH₂(CH₂C₆H₄C(CH₃)3)2⁽¹⁺⁾*PF₆^(1-)*[Ni((C₆H₄NCHC₆H₃(O)O(C₂H₄O)2)2)]=[Ni(C₆H₄NCHC₆H₃O₂(C₂H₄O)2)2]H₂N(CH₂C₆H₄C(CH₃)3)2PF₆
• CAS No.: 1098226-80-2
• Molecular Formula: C₂₂H₃₂N*C₃₄H₃₂N₂NiO₈*F₆P
• Molecular Weight: 1110.79
• Mol file: 1098226-80-2.mol

Synonyms:

Chemical Property of NH₂(CH₂C₆H₄C(CH₃)3)2⁽¹⁺⁾*PF₆^(1-)*[Ni((C₆H₄NCHC₆H₃(O)O(C₂H₄O)2)2)]=[Ni(C₆H₄NCHC₆H₃O₂(C₂H₄O)2)2]H₂N(CH₂C₆H₄C(CH₃)3)2PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of NH₂(CH₂C₆H₄C(CH₃)3)2⁽¹⁺⁾*PF₆^(1-)*[Ni((C₆H₄NCHC₆H₃(O)O(C₂H₄O)2)2)]=[Ni(C₆H₄NCHC₆H₃O₂(C₂H₄O)2)2]H₂N(CH₂C₆H₄C(CH₃)3)2PF₆

There total 1 articles about NH₂(CH₂C₆H₄C(CH₃)3)2⁽¹⁺⁾*PF₆^(1-)*[Ni((C₆H₄NCHC₆H₃(O)O(C₂H₄O)2)2)]=[Ni(C₆H₄NCHC₆H₃O₂(C₂H₄O)2)2]H₂N(CH₂C₆H₄C(CH₃)3)2PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

H2N(CH2C6H4C(CH3)3)2(1+)*PF6(1-)=[H2N(CH2C6H4C(CH3)3)2]PF6 (202849-36-3) + Ba(2+)*2ClO4(1-)*(C6H4NCHC6H3(OH)O(C2H4O)2)2=Ba(ClO4)2((C6H4NCHC6H3(OH)O(C2H4O)2)2) + nickel(II) acetate tetrahydrate (6018-89-9) → NH2(CH2C6H4C(CH3)3)2(1+)*PF6(1-)*[Ni((C6H4NCHC6H3(O)O(C2H4O)2)2)]=[Ni(C6H4NCHC6H3O2(C2H4O)2)2]H2N(CH2C6H4C(CH3)3)2PF6 (1098226-80-2)

Guidance literature:

With Na₂SO₄; In methanol; water; acetonitrile; N2, a soln of Na compd. (water/CH3CN) added to a soln. of Ba and P compds. (CH3CN), stirred for 2 h, a soln. of Ni salt (CH3CN/methanol) added, stirred for 12 h; filtered, solvent evapd. (vac.), dissolved (CH3CN), chromy. (SiO2, CH2Cl2/methanol), solvent evapd. (vac.); elem. anal.;

DOI:10.1002/ejic.200700208

upstream raw materials:

H₂N(CH₂C₆H₄C(CH₃)3)2⁽¹⁺⁾*PF₆^(1-)=[H₂N(CH₂C₆H₄C(CH₃)3)2]PF₆

nickel(II) acetate tetrahydrate