2-hydroxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone dimer, diacetate

Base Information

Chemical Name:2-hydroxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone dimer, diacetate
CAS No.:168916-92-5
Molecular Formula:C₅₆H₇₆O₆Sn₂
Molecular Weight:1082.64
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-hydroxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone dimer, diacetate

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Technology Process of 2-hydroxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone dimer, diacetate

There total 1 articles about 2-hydroxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone dimer, diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: [4-(tri-n-butylstannyl)phenyl]lithium

: 108-24-7
acetic anhydride

: 6383-11-5
benzocyclobutene-1,2-dione

: 168916-96-9
2-acetoxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone

: 168916-92-5
2-hydroxy-2-[4'-(tri-n-butylstannyl)phenyl]benzocyclobutenone dimer, diacetate

Guidance literature:: In tetrahydrofuran; stirring at -78°C for 1 h, quenching with Ac2O; chromatographic workup; elem. anal.;
DOI:10.1021/ja00117a009