all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al

Base Information

Chemical Name:all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al
CAS No.:119479-35-5
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al

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Technology Process of all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al

There total 6 articles about all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: C₁₅H₂₃N

: 62924-16-7,119479-35-5,121524-15-0,121570-40-9
all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al

Guidance literature:: C₁₅H₂₃N; With diisobutylaluminium hydride; In toluene; at -60 ℃; for 0.5h; Inert atmosphere;

With silica gel; In toluene; at -60 - -30 ℃; for 1h; Inert atmosphere;
DOI:10.1124/mol.114.096560

Reference yield:

: 82648-70-2
diethyl (3-cyano-2-methyl-2-trans-propenyl)phosphonate

: 62924-16-7,119479-35-5,121524-15-0,121570-40-9
all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 °C

1.2: 1 h / 0 - 20 °C

2.1: diisobutylaluminium hydride / toluene / 0.5 h / -60 °C / Inert atmosphere

2.2: 1 h / -60 - -30 °C / Inert atmosphere

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; toluene; 1.1: |Wittig-Horner Reaction / 1.2: |Wittig-Horner Reaction;
DOI:10.1124/mol.114.096560

Reference yield:

: 57576-59-7
3,7-dimethyl-octa-1,6-dien-1-yl acetate

: 62924-16-7,119479-35-5,121524-15-0,121570-40-9
all-trans-5-(2,2,6-Trimethyl-cyclohexyl)-3-methyl-pentadien-(2,4)-al

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphoric acid / toluene / 3 h / Reflux

2.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 °C

2.2: 1 h / 0 - 20 °C

3.1: diisobutylaluminium hydride / toluene / 0.5 h / -60 °C / Inert atmosphere

3.2: 1 h / -60 - -30 °C / Inert atmosphere

With phosphoric acid; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; toluene; 2.1: |Wittig-Horner Reaction / 2.2: |Wittig-Horner Reaction;
DOI:10.1124/mol.114.096560