cis-dichlorobis(2,6-xylyl isocynide)nickel(II)

Base Information

Chemical Name:cis-dichlorobis(2,6-xylyl isocynide)nickel(II)
CAS No.:126076-72-0
Molecular Formula:C₁₈H₁₈Cl₂N₂Ni
Molecular Weight:391.95
Hs Code.:

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Chemical Property of cis-dichlorobis(2,6-xylyl isocynide)nickel(II)

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Technology Process of cis-dichlorobis(2,6-xylyl isocynide)nickel(II)

There total 1 articles about cis-dichlorobis(2,6-xylyl isocynide)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 14264-16-5,53996-95-5,62075-39-2,39716-73-9
bis(triphenylphosphine)nickel(II) chloride

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: 126076-72-0,139068-38-5
cis-dichlorobis(2,6-xylyl isocynide)nickel(II)

Guidance literature:: In dichloromethane; to a soln. of NiCl2(PPh3)2 in CH2Cl2 is added 2,6-xylyl isocyanide at room temp.; after 1 h the soln. is filtered und the solvent is removed in vac., crystn. from CH2Cl2 and hexane; elem. anal.;
DOI:10.1246/bcsj.64.3376

Reference yield: 65.0%

: 126076-72-0,139068-38-5
cis-dichlorobis(2,6-xylyl isocynide)nickel(II)

: 119072-54-7,2769-71-3
2,6-dimethylphenyl isonitrile

: mercury

: {Ni((CH₃)2C₆H₃NC)4HgCl₂}2

Guidance literature:: In acetonitrile; a mixt. of cis-NiCl2(2,6-Me2C6H3NC)2, 2,6-xylyl isocyanide and Hg is stirred for 2.5 h at room temp.,ppt.; the organic layer is dried, residue is extd. with benzene, the solvent is concd., hexane added, giving crystals; elem. anal.;
DOI:10.1246/bcsj.64.3376

Reference yield:

: 126076-72-0,139068-38-5
cis-dichlorobis(2,6-xylyl isocynide)nickel(II)

: 139010-70-1
dibromobis[2-(isocyano-κC)-1,3-dimethylbenzene]nickel

Guidance literature:: With KBr; In not given; is prepared from a metathesis of cis-NiCl2(2,6-Me2C6H3NC)2 with KBr; elem. anal.;
DOI:10.1246/bcsj.64.3376