(2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh

Base Information

Chemical Name:(2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh
CAS No.:1180491-89-7
Molecular Formula:C₂₆H₂₃BrHgNP
Molecular Weight:660.943
Hs Code.:

(2-BrHgC<sub>6</sub>H<sub>4</sub>)Ph<sub>2</sub>P=N-(R,S)-CHMePh

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Chemical Property of (2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh

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Technology Process of (2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh

There total 1 articles about (2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 52826-43-4,52918-35-1
[Ph₃P-NH-(R,S)-CHMePh]Br

: mercury dichloride

: 1180491-89-7
(2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; (N2); 1.6 M BuLi inn hexane was added to suspn. of phosphonic salt in Et2O at -84°C, allowed to warm to room temp., stirred for 30 min, HgCl2 was added, stirred for 1 h; evapd., extd. with CH2Cl2, filtered, crystd. with Et2O at -20°C, elem. anal.;
DOI:10.1016/j.ica.2009.04.024

Reference yield: 64.0%

: 53514-38-8
tetramethylammonium tetrachloroaurate(III)

: 1180491-89-7
(2-BrHgC₆H₄)Ph₂P=N-(R,S)-CHMePh

: 75-57-0
tetramethlyammonium chloride

: 1180491-93-3,1180492-64-1
(2-Cl₂AuC₆H₄)Ph₂P=N-(R,S)-CHMePh

Guidance literature:: In acetonitrile; (dark); mercury complex, Me4N(AuCl4) and Me4NCl were added to MeCN, stirred for 48 h; evapd., extd. with CH2Cl2, filtered, Et2O was added to fitrate, crystd. at -20°C, elem. anal.;
DOI:10.1016/j.ica.2009.04.024