C₂₅H₂₅N₉O

Base Information

Chemical Name:C₂₅H₂₅N₉O
CAS No.:1207358-77-7
Molecular Formula:C₂₅H₂₅N₉O
Molecular Weight:467.533
Hs Code.:

C<sub>25</sub>H<sub>25</sub>N<sub>9</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₅N₉O

Chemical Property:

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Technology Process of C₂₅H₂₅N₉O

There total 8 articles about C₂₅H₂₅N₉O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207370-38-4
tert-butyl 2-chloro-4-morpholino-5,6-dihydropyrido[3,4-d]pyrimidine-7(8H)-carboxylate

: 1207358-77-7
C₂₅H₂₅N₉O

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; potassium acetate / acetonitrile; water / 0.25 h / Microwave irradiation; Heating; Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / Microwave irradiation; Heating; Inert atmosphere

4: tin(II) chloride dihdyrate / ethanol / 1 h / Inert atmosphere; Reflux

5: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium diacetate / 1,4-dioxane / 0.67 h / Microwave irradiation; Heating; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tin(II) chloride dihdyrate; potassium acetate; palladium diacetate; sodium carbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; trifluoroacetic acid; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: |Suzuki Coupling;
DOI:10.1021/ml3003132

Reference yield:

: 1415797-55-5
tert-butyl 4-morpholino-2-(4-nitrophenyl)-5,6-dihydropyrido[3,4-d]pyrimidine-7(8H)-carboxylate

: 1207358-77-7
C₂₅H₂₅N₉O

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.5 h / Microwave irradiation; Heating; Inert atmosphere

3: tin(II) chloride dihdyrate / ethanol / 1 h / Inert atmosphere; Reflux

4: caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; palladium diacetate / 1,4-dioxane / 0.67 h / Microwave irradiation; Heating; Inert atmosphere

With tin(II) chloride dihdyrate; palladium diacetate; caesium carbonate; N-ethyl-N,N-diisopropylamine; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; trifluoroacetic acid; In 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml3003132

Reference yield:

: 1415797-56-6
4-(2-(4-nitrophenyl)-7-(pyrimidin-2-yl)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidin-4-yl)morpholine

: 1207358-77-7
C₂₅H₂₅N₉O

Guidance literature:: Multi-step reaction with 2 steps

1: tin(II) chloride dihdyrate / ethanol / 1 h / Inert atmosphere; Reflux

2: caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; palladium diacetate / 1,4-dioxane / 0.67 h / Microwave irradiation; Heating; Inert atmosphere

With tin(II) chloride dihdyrate; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; ethanol;
DOI:10.1021/ml3003132