(HOOCC₆H₄)2C₁₃H₆O

Base Information

Chemical Name:(HOOCC₆H₄)2C₁₃H₆O
CAS No.:1313187-37-9
Molecular Formula:C₂₇H₁₆O₅
Molecular Weight:420.421
Hs Code.:

(HOOCC<sub>6</sub>H<sub>4</sub>)2C<sub>13</sub>H<sub>6</sub>O

Synonyms:

Suppliers and Price of (HOOCC₆H₄)2C₁₃H₆O

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (HOOCC₆H₄)2C₁₃H₆O

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of (HOOCC₆H₄)2C₁₃H₆O

There total 4 articles about (HOOCC₆H₄)2C₁₃H₆O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313187-44-8
C₃₁H₂₄O₅

: 1313187-37-9
(HOOCC₆H₄)2C₁₃H₆O

Guidance literature:: C₃₁H₂₄O₅; With tetrabutylammomium bromide; sodium hydroxide; In tetrahydrofuran; water; at 70 ℃; for 6h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; pH=2 - 3;
DOI:10.1002/anie.201007277

Reference yield:

: 1314484-70-2
dimethyl 4,4'-(9-oxo-9H-fluorene-2,7-diyl)dibenzoate

: 1313187-37-9
(HOOCC₆H₄)2C₁₃H₆O

Guidance literature:: dimethyl 4,4'-(9-oxo-9H-fluorene-2,7-diyl)dibenzoate; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran;

With perchloric acid; In tetrahydrofuran;
DOI:10.1039/c0jm04214e

Reference yield:

: 14348-75-5
2,7-dibromofluorene-9-one

: 195062-62-5
ethyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 1313187-37-9
(HOOCC₆H₄)2C₁₃H₆O

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; sodium carbonate / toluene / 6 h / 80 °C / Inert atmosphere

2.1: tetrabutylammomium bromide; sodium hydroxide / tetrahydrofuran; water / 6 h / 70 °C

2.2: 20 °C / pH 2 - 3

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; sodium carbonate; sodium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1002/anie.201007277