9-acetyl-2-benzoylcarbazole

Base Information

• Chemical Name: 9-acetyl-2-benzoylcarbazole
• CAS No.: 125424-77-3
• Molecular Formula: C₂₁H₁₅NO₂
• Molecular Weight: 313.356
• Mol file: 125424-77-3.mol

Synonyms:

Chemical Property of 9-acetyl-2-benzoylcarbazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 9-acetyl-2-benzoylcarbazole

There total 5 articles about 9-acetyl-2-benzoylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

(9H-carbazol-2-yl)(phenyl)methanone (23592-78-1) + acetic anhydride (108-24-7) → 9-acetyl-2-benzoylcarbazole (125424-77-3)

Guidance literature:

With sulfuric acid;

DOI:10.1016/S0040-4020(01)89239-5

Reference yield:

9-benzoyl-9H-carbazole (19264-68-7) → 9-acetyl-2-benzoylcarbazole (125424-77-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 60 percent / AlCl₃ / CS₂ / Heating

2: 85 percent / 10percent potassium hydroxide / ethanol / 1 h

3: 30 percent / H₂SO₄

With potassium hydroxide; aluminium trichloride; sulfuric acid; In carbon disulfide; ethanol;

DOI:10.1016/S0040-4020(01)89239-5

Reference yield:

2,9-dibenzoylcarbazole (23592-77-0) → 9-acetyl-2-benzoylcarbazole (125424-77-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / 10percent potassium hydroxide / ethanol / 1 h

2: 30 percent / H₂SO₄

With potassium hydroxide; sulfuric acid; In ethanol;

DOI:10.1016/S0040-4020(01)89239-5

upstream raw materials:

9-acetylcarbazole

benzoyl chloride

(9H-carbazol-2-yl)(phenyl)methanone

acetic anhydride

Downstream raw materials:

(9H-carbazol-2-yl)(phenyl)methanone

1-(7-benzoyl-carbazol-3-yl)-ethanone

1-(7,9-dibenzoyl-carbazol-3-yl)-ethanone

1-(7-benzoyl-9-methyl-carbazol-3-yl)-ethanone