4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile

Base Information

Chemical Name:4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile
CAS No.:33721-67-4
Molecular Formula:C₁₄H₁₀N₂O
Molecular Weight:222.246
Hs Code.:
European Community (EC) Number:667-127-7
NSC Number:119179
Nikkaji Number:J1.529.822G

Synonyms:33721-67-4;4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile;4-((2-Hydroxybenzylidene)amino)benzonitrile;4-[(2-hydroxyphenyl)methylideneamino]benzonitrile;NSC119179;SCHEMBL3365845;STK948949;AKOS004906540;AKOS005641202;NSC-119179;4-(2-Hydroxybenzylideneamino)benzonitrile;BS-10386;ALPHA-(4-CYANOPHENYLIMINO)-O-CRESOL;CS-0366132;SR-01000201561;SR-01000201561-1;4-{[(E)-(2-hydroxyphenyl)methylidene]amino}benzonitrile

Suppliers and Price of 4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile

Chemical Property:

Vapor Pressure:2.67E-07mmHg at 25°C
Boiling Point:421.1°C at 760 mmHg
Flash Point:208.5°C
Density:1.23g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:222.079312947
Heavy Atom Count:17
Complexity:309

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C=NC2=CC=C(C=C2)C#N)O

Technology Process of 4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile

There total 1 articles about 4-{[(1E)-(2-hydroxyphenyl)methylene]amino}benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 90-02-8
salicylaldehyde

: 873-74-5
4-Aminobenzonitrile

: 33721-67-4,117909-27-0
4-(2-hydroxybenzylideneamino)benzonitrile

Guidance literature:: In ethanol; at 25 ℃; for 24h;
DOI:10.1016/j.jphotochem.2017.02.016

Reference yield: 75.0%

: 33721-67-4,117909-27-0
4-(2-hydroxybenzylideneamino)benzonitrile

: 873-74-5
4-Aminobenzonitrile

Guidance literature:: With tetrabutylammomium bromide; water; In dimethylsulfoxide-d6; for 24h;
DOI:10.1039/d1ra07677a

Reference yield: 44.0%

: Fe₂Cl₄*3C₄H₈O

: 33721-67-4,117909-27-0
4-(2-hydroxybenzylideneamino)benzonitrile

: 108-88-3,15644-74-3,16713-13-6
toluene

: Fe(OC₆H₄CHNC₆H₄CN)2*0.33C₇H₈

Guidance literature:: With NaH; In tetrahydrofuran; byproducts: NaCl; (Ar, Schlenk) benzonitrile-compound was stirred with NaH in THF for 6 h,the suspn. was filtered into a soln. of Fe2Cl4*3THF in THF at -78.degre e.C, stirred for 12 h at ambient temp.; volatiles were removed in vac., the solid was extd. into CH2Cl2, filtered, concd., filtered, recrystd. from boiling toluene; elem. anal.;
DOI:10.1039/b905706d