chloro(η2-diphenylbutadiyne)tris(trimethylphosphine)cobalt

Base Information

• Chemical Name: chloro(η2-diphenylbutadiyne)tris(trimethylphosphine)cobalt
• CAS No.: 149073-63-2
• Molecular Formula: C₂₅H₃₇ClCoP₃
• Molecular Weight: 524.936
• Mol file: 149073-63-2.mol

Synonyms:

Chemical Property of chloro(η2-diphenylbutadiyne)tris(trimethylphosphine)cobalt

Chemical Property:

Purity/Quality:

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Technology Process of chloro(η2-diphenylbutadiyne)tris(trimethylphosphine)cobalt

There total 1 articles about chloro(η2-diphenylbutadiyne)tris(trimethylphosphine)cobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

chlorotris(trimethylphosphane)cobalt(I) (55516-89-7) + 1,4-diphenyl-1,3-butadiyne (886-66-8) → chloro(η2-diphenylbutadiyne)tris(trimethylphosphine)cobalt (149073-63-2)

Guidance literature:

In tetrahydrofuran; combining CoCl(P(CH3)3)3 (1.84 mmol) in THF with diphenylbutadiyne (1.85 mmol) in THF at -70°C; warming to 20°C;; filtering after 12 h; concg. in vac.; crystn. at -20°C after 10 d; elem. anal.;;

DOI:10.1016/S0020-1693(00)91458-0

upstream raw materials:

chlorotris(trimethylphosphane)cobalt(I)

1,4-diphenyl-1,3-butadiyne