C₇₀H₅₆N₆O₅

Base Information

Chemical Name:C₇₀H₅₆N₆O₅
CAS No.:126442-79-3
Molecular Formula:C₇₀H₅₆N₆O₅
Molecular Weight:1061.25
Hs Code.:

C<sub>70</sub>H<sub>56</sub>N<sub>6</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₇₀H₅₆N₆O₅

Chemical Property:

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Technology Process of C₇₀H₅₆N₆O₅

There total 18 articles about C₇₀H₅₆N₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126442-64-6
3-carbomethoxy-4-(2,5-dimethoxyphenyl)-3-butenoic acid

: 126442-79-3
C₇₀H₅₆N₆O₅

Guidance literature:: Multi-step reaction with 15 steps

1: hydrogen / 5percent palladium on carbon / methanol / 20 h / 2068.6 Torr

2: 89 percent / polyphosphoric acid / 0.33 h / 85 °C

3: 85 percent / hydrogen / 10percent palladium on carbon / acetic acid / 1 h / 40 °C / 2585.7 Torr

4: 61 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 72 h / 40 °C

5: 81 percent / ceric ammonium nitrate / H₂O; acetonitrile / 0.17 h / Ambient temperature

6: 88 percent / toluene / 0.17 h / Ambient temperature

7: 85 percent / 10 percent methanolic KOH / acetone

8: 90 percent / hydroquinone / solid / 30 h / 140 °C

9: sodium methoxide / methanol / 24 h / Ambient temperature

10: activated manganese dioxide / CH₂Cl₂ / 120 h

11: 0.02M aq. sodium dithionit / tetrahydrofuran

12: 80 percent / potassium carbonate / acetone / 24 h

13: 95 percent / 10percent aq. potassium hydroxide / tetrahydrofuran; methanol / 24 h

14: thionyl chloride, pyridine / toluene / 0.08 h

15: pyridine / CHCl₃

With pyridine; manganese(IV) oxide; potassium hydroxide; thionyl chloride; sodium dithionite; PPA; ammonium cerium(IV) nitrate; hydrogen; sodium methylate; potassium carbonate; hydroquinone; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; acetic acid; acetone; toluene; acetonitrile; benzene;
DOI:10.1016/S0040-4020(01)85157-7

Reference yield:

: 76117-16-3
methyl 1,2,3,4-tetrahydro-5,8-dimethoxy-4-oxonaphthalene-2-carboxylate

: 126442-79-3
C₇₀H₅₆N₆O₅

Guidance literature:: Multi-step reaction with 13 steps

1: 85 percent / hydrogen / 10percent palladium on carbon / acetic acid / 1 h / 40 °C / 2585.7 Torr

2: 61 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 72 h / 40 °C

3: 81 percent / ceric ammonium nitrate / H₂O; acetonitrile / 0.17 h / Ambient temperature

4: 88 percent / toluene / 0.17 h / Ambient temperature

5: 85 percent / 10 percent methanolic KOH / acetone

6: 90 percent / hydroquinone / solid / 30 h / 140 °C

7: sodium methoxide / methanol / 24 h / Ambient temperature

8: activated manganese dioxide / CH₂Cl₂ / 120 h

9: 0.02M aq. sodium dithionit / tetrahydrofuran

10: 80 percent / potassium carbonate / acetone / 24 h

11: 95 percent / 10percent aq. potassium hydroxide / tetrahydrofuran; methanol / 24 h

12: thionyl chloride, pyridine / toluene / 0.08 h

13: pyridine / CHCl₃

With pyridine; manganese(IV) oxide; potassium hydroxide; thionyl chloride; sodium dithionite; ammonium cerium(IV) nitrate; hydrogen; sodium methylate; potassium carbonate; hydroquinone; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; acetic acid; acetone; toluene; acetonitrile; benzene;
DOI:10.1016/S0040-4020(01)85157-7

Reference yield:

: 2-[1-(2,5-Dimethoxy-phenyl)-meth-(E)-ylidene]-succinic acid dimethyl ester

: 126442-79-3
C₇₀H₅₆N₆O₅

Guidance literature:: Multi-step reaction with 16 steps

1: 4M aq. HCl

2: hydrogen / 5percent palladium on carbon / methanol / 20 h / 2068.6 Torr

3: 89 percent / polyphosphoric acid / 0.33 h / 85 °C

4: 85 percent / hydrogen / 10percent palladium on carbon / acetic acid / 1 h / 40 °C / 2585.7 Torr

5: 61 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 72 h / 40 °C

6: 81 percent / ceric ammonium nitrate / H₂O; acetonitrile / 0.17 h / Ambient temperature

7: 88 percent / toluene / 0.17 h / Ambient temperature

8: 85 percent / 10 percent methanolic KOH / acetone

9: 90 percent / hydroquinone / solid / 30 h / 140 °C

10: sodium methoxide / methanol / 24 h / Ambient temperature

11: activated manganese dioxide / CH₂Cl₂ / 120 h

12: 0.02M aq. sodium dithionit / tetrahydrofuran

13: 80 percent / potassium carbonate / acetone / 24 h

14: 95 percent / 10percent aq. potassium hydroxide / tetrahydrofuran; methanol / 24 h

15: thionyl chloride, pyridine / toluene / 0.08 h

16: pyridine / CHCl₃

With pyridine; hydrogenchloride; manganese(IV) oxide; potassium hydroxide; thionyl chloride; sodium dithionite; PPA; ammonium cerium(IV) nitrate; hydrogen; sodium methylate; potassium carbonate; hydroquinone; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; acetic acid; acetone; toluene; acetonitrile; benzene;
DOI:10.1016/S0040-4020(01)85157-7