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Technology Process of (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl

(((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl

Base Information
  • Chemical Name:(((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl
  • CAS No.:1207199-72-1
  • Molecular Formula:C41H50ClGeN2P
  • Molecular Weight:709.878
  • Hs Code.:
(((CH<sub>3</sub>)2CH)2C<sub>6</sub>H<sub>3</sub>NC(CH<sub>3</sub>)C(P(C<sub>6</sub>H<sub>5</sub>)2)C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)GeCl

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Chemical Property of (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl
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Technology Process of (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl

There total 1 articles about (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

germanium(II) chloride-dioxane complex

germanium(II) chloride-dioxane complex

(((CH<sub>3</sub>)2CH)2C<sub>6</sub>H<sub>3</sub>NC(CH<sub>3</sub>)C(P(C<sub>6</sub>H<sub>5</sub>)2)C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)Li(O(C<sub>2</sub>H<sub>5</sub>)2)
1207199-70-9

(((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)Li(O(C2H5)2)

(((CH<sub>3</sub>)2CH)2C<sub>6</sub>H<sub>3</sub>NC(CH<sub>3</sub>)C(P(C<sub>6</sub>H<sub>5</sub>)2)C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)GeCl

(((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl

(((CH<sub>3</sub>)2CH)2C<sub>6</sub>H<sub>3</sub>NC(CH<sub>3</sub>)C(P(C<sub>6</sub>H<sub>5</sub>)2)C(CH<sub>3</sub>)NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)GeCl
1207199-72-1

(((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl

Guidance literature:
In diethyl ether; under N2 or Ar; suspn. of Li compd. in ether added to cooled (-30°C) suspn. of Ge complex in ether using L-bent tube; stirred at room temp. overnight; filtered (Celite); volatiles removed from filtrate; n-hexane added; stirred for ca. 30 min; ppt. collected by filtration; additional crop obtained from filtrate by crystn. at room temp. for 1 d; elem. anal.;
DOI:10.1039/b915403e
upstream raw materials:

(((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)Li(O(C2H5)2)

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