(((CH₃)2CH)2C₆H₃NC(CH₃)C(P(C₆H₅)2)C(CH₃)NC₆H₃(CH(CH₃)2)2)GeCl

Base Information

• Chemical Name: (((CH₃)2CH)2C₆H₃NC(CH₃)C(P(C₆H₅)2)C(CH₃)NC₆H₃(CH(CH₃)2)2)GeCl
• CAS No.: 1207199-72-1
• Molecular Formula: C₄₁H₅₀ClGeN₂P
• Molecular Weight: 709.878
• Mol file: 1207199-72-1.mol

Synonyms:

Chemical Property of (((CH₃)2CH)2C₆H₃NC(CH₃)C(P(C₆H₅)2)C(CH₃)NC₆H₃(CH(CH₃)2)2)GeCl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (((CH₃)2CH)2C₆H₃NC(CH₃)C(P(C₆H₅)2)C(CH₃)NC₆H₃(CH(CH₃)2)2)GeCl

There total 1 articles about (((CH₃)2CH)2C₆H₃NC(CH₃)C(P(C₆H₅)2)C(CH₃)NC₆H₃(CH(CH₃)2)2)GeCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

germanium(II) chloride-dioxane complex + (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)Li(O(C2H5)2) (1207199-70-9) → (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl + (((CH3)2CH)2C6H3NC(CH3)C(P(C6H5)2)C(CH3)NC6H3(CH(CH3)2)2)GeCl (1207199-72-1)

Guidance literature:

In diethyl ether; under N2 or Ar; suspn. of Li compd. in ether added to cooled (-30°C) suspn. of Ge complex in ether using L-bent tube; stirred at room temp. overnight; filtered (Celite); volatiles removed from filtrate; n-hexane added; stirred for ca. 30 min; ppt. collected by filtration; additional crop obtained from filtrate by crystn. at room temp. for 1 d; elem. anal.;

DOI:10.1039/b915403e

upstream raw materials:

(((CH₃)2CH)2C₆H₃NC(CH₃)C(P(C₆H₅)2)C(CH₃)NC₆H₃(CH(CH₃)2)2)Li(O(C₂H₅)2)