1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom

Base Information

Chemical Name:1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom
CAS No.:158443-24-4
Molecular Formula:C₁₇H₁₂CrO₅
Molecular Weight:348.275
Hs Code.:

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Chemical Property of 1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom

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Technology Process of 1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom

There total 1 articles about 1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 16605-99-5
biphenyl-2-carboxylic acid methyl ester

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 158443-24-4,73527-06-7
1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom

Guidance literature:: In n-heptane; dibutyl ether; mixture was refluxed for 48 h under Ar; filtered in hot, filtrate was cooled, ppt. collected, washed with petroleum ether, dried in vac., chromy.; elem. anal.;
DOI:10.1007/BF00938733

Reference yield: 91.0%

: 158443-24-4,73527-06-7
1,1'-Biphenyl-2-carbonsaeuremethylester-tricarbonylchrom

: 68866-65-9
1,1'-Biphenyl-2-carbonsaeure-tricarbonylchrom

Guidance literature:: With potassium hydroxide; In methanol; water; the soln. was stirred at 60°C for 2 h, allowed to stay at room temp. for overnight under Ar; partially evapd. in vac., HCl/H2O was added, ppt. was collected, washedwith CH2Cl2, dried in vac.; elem. anal.;
DOI:10.1007/BF00938733