Technology Process of C51H57NO3
There total 6 articles about C51H57NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / methanol; chloroform / 24 h / Inert atmosphere; Reflux
2: hydrogenchloride / 1,4-dioxane / 0.17 h
3: potassium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux
With
hydrogenchloride; potassium carbonate;
In
1,4-dioxane; methanol; chloroform; acetonitrile;
DOI:10.1002/chir.20994
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / N,N-dimethyl-formamide / Inert atmosphere
2: potassium carbonate / methanol; chloroform / 24 h / Inert atmosphere; Reflux
3: hydrogenchloride / 1,4-dioxane / 0.17 h
4: potassium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux
With
hydrogenchloride; potassium carbonate; triethylamine;
In
1,4-dioxane; methanol; chloroform; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chir.20994
- Guidance literature:
-
Multi-step reaction with 2 steps
1: phosphorus tribromide / toluene / 0.83 h / 20 °C / Inert atmosphere; Cooling with ice
2: potassium carbonate / acetonitrile / 48 h / Inert atmosphere; Reflux
With
phosphorus tribromide; potassium carbonate;
In
toluene; acetonitrile;
DOI:10.1002/chir.20994
