C₄₁H₆₀O₅

Base Information

Chemical Name:C₄₁H₆₀O₅
CAS No.:1315381-22-6
Molecular Formula:C₄₁H₆₀O₅
Molecular Weight:632.924
Hs Code.:

C<sub>41</sub>H<sub>60</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₆₀O₅

Chemical Property:

Purity/Quality:

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Technology Process of C₄₁H₆₀O₅

There total 16 articles about C₄₁H₆₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1315380-97-2
(17Z)-3β-acetoxy-5β,6β-epoxypregn-17(20)-ene

: 1315381-24-8
C₄₁H₆₀O₅

: 1315381-22-6
C₄₁H₆₀O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: boron trifluoride diethyl etherate; sodium cyanoborohydride / tetrahydrofuran / 2.58 h / 50 °C

2.1: methanol; sodium hydroxide / 4 h / 25 °C

3.1: sodium hydride / tetrahydrofuran; hexanes; N,N-dimethyl-formamide / 0.5 h / 25 °C

3.2: 48 h / 25 °C / light protection

4.1: tert.-butylhydroperoxide; selenium(IV) oxide / decane; dichloromethane / 4 h / 0 °C

5.1: Dess-Martin periodane / dichloromethane / 2 h / 25 °C

6.1: aluminum (III) chloride / tetrahydrofuran; diethyl ether / 0.17 h / -30 °C

6.2: 0.33 h / -30 °C

7.1: 1,2-dimethoxyethane; potassium hydride / hexanes / 1 h / Reflux

7.2: -20 - -10 °C

8.1: ozone / dichloromethane / -78 °C

8.2: -78 - 20 °C

9.1: n-butyllithium / hexanes; diethyl ether / 25 °C

9.2: -78 - 25 °C

10.1: diisobutylaluminium hydride / diethyl ether / 3 h / -78 °C

10.2: -78 - 20 °C

11.1: 4-methyl-morpholine; tert.-butylhydroperoxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 25 °C

With 4-methyl-morpholine; methanol; tert.-butylhydroperoxide; selenium(IV) oxide; aluminum (III) chloride; osmium(VIII) oxide; n-butyllithium; 1,2-dimethoxyethane; boron trifluoride diethyl etherate; potassium hydride; sodium hydride; diisobutylaluminium hydride; sodium cyanoborohydride; Dess-Martin periodane; ozone; sodium hydroxide; In tetrahydrofuran; hexanes; diethyl ether; decane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Williamson synthesis / 3.2: Williamson synthesis / 7.1: oxy-Cope rearrangement;
DOI:10.1002/chem.201100503

Reference yield:

: 1315380-98-3
(17Z)-3β-acetoxy-5α-pregn-17(20)-ene-6β-ol

: 1315381-24-8
C₄₁H₆₀O₅

: 1315381-22-6
C₄₁H₆₀O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: methanol; sodium hydroxide / 4 h / 25 °C

2.1: sodium hydride / tetrahydrofuran; hexanes; N,N-dimethyl-formamide / 0.5 h / 25 °C

2.2: 48 h / 25 °C / light protection

3.1: tert.-butylhydroperoxide; selenium(IV) oxide / decane; dichloromethane / 4 h / 0 °C

4.1: Dess-Martin periodane / dichloromethane / 2 h / 25 °C

5.1: aluminum (III) chloride / tetrahydrofuran; diethyl ether / 0.17 h / -30 °C

5.2: 0.33 h / -30 °C

6.1: 1,2-dimethoxyethane; potassium hydride / hexanes / 1 h / Reflux

6.2: -20 - -10 °C

7.1: ozone / dichloromethane / -78 °C

7.2: -78 - 20 °C

8.1: n-butyllithium / hexanes; diethyl ether / 25 °C

8.2: -78 - 25 °C

9.1: diisobutylaluminium hydride / diethyl ether / 3 h / -78 °C

9.2: -78 - 20 °C

10.1: 4-methyl-morpholine; tert.-butylhydroperoxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 25 °C

With 4-methyl-morpholine; methanol; tert.-butylhydroperoxide; selenium(IV) oxide; aluminum (III) chloride; osmium(VIII) oxide; n-butyllithium; 1,2-dimethoxyethane; potassium hydride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; ozone; sodium hydroxide; In tetrahydrofuran; hexanes; diethyl ether; decane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Williamson synthesis / 2.2: Williamson synthesis / 6.1: oxy-Cope rearrangement;
DOI:10.1002/chem.201100503

Reference yield:

: 1315381-08-8
(17Z)-5α-pregn-17(20)-ene-3β,6β-diol

: 1315381-24-8
C₄₁H₆₀O₅

: 1315381-22-6
C₄₁H₆₀O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / tetrahydrofuran; hexanes; N,N-dimethyl-formamide / 0.5 h / 25 °C

1.2: 48 h / 25 °C / light protection

2.1: tert.-butylhydroperoxide; selenium(IV) oxide / decane; dichloromethane / 4 h / 0 °C

3.1: Dess-Martin periodane / dichloromethane / 2 h / 25 °C

4.1: aluminum (III) chloride / tetrahydrofuran; diethyl ether / 0.17 h / -30 °C

4.2: 0.33 h / -30 °C

5.1: 1,2-dimethoxyethane; potassium hydride / hexanes / 1 h / Reflux

5.2: -20 - -10 °C

6.1: ozone / dichloromethane / -78 °C

6.2: -78 - 20 °C

7.1: n-butyllithium / hexanes; diethyl ether / 25 °C

7.2: -78 - 25 °C

8.1: diisobutylaluminium hydride / diethyl ether / 3 h / -78 °C

8.2: -78 - 20 °C

9.1: 4-methyl-morpholine; tert.-butylhydroperoxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 25 °C

With 4-methyl-morpholine; tert.-butylhydroperoxide; selenium(IV) oxide; aluminum (III) chloride; osmium(VIII) oxide; n-butyllithium; 1,2-dimethoxyethane; potassium hydride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; ozone; In tetrahydrofuran; hexanes; diethyl ether; decane; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Williamson synthesis / 1.2: Williamson synthesis / 5.1: oxy-Cope rearrangement;
DOI:10.1002/chem.201100503