C₂₀H₂₃N₅O₂

Base Information

Chemical Name:C₂₀H₂₃N₅O₂
CAS No.:1415838-69-5
Molecular Formula:C₂₀H₂₃N₅O₂
Molecular Weight:365.435
Hs Code.:

C<sub>20</sub>H<sub>23</sub>N<sub>5</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₀H₂₃N₅O₂

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Technology Process of C₂₀H₂₃N₅O₂

There total 3 articles about C₂₀H₂₃N₅O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1415838-58-2
8-(butylamino)-7-(2-(2,6-dimethylphenyl)-2-oxoethyl)-3-methyl-1H-purine-2,6(3H,7H)-dione

: 1415838-69-5
C₂₀H₂₃N₅O₂

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 175 ℃; for 6h; Sealed tube; Inert atmosphere; Schlenk technique;
DOI:10.1021/jm301187e

Reference yield:

: 2633-42-3
2-bromo-2',6'-dimethylacetophenone

: 1415838-69-5
C₂₀H₂₃N₅O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.08 h / 25 °C / Inert atmosphere; Schlenk technique

1.2: 2 h / 110 °C / Inert atmosphere; Schlenk technique

2.1: ethanol / 2 h / 175 °C / Sealed tube; Schlenk technique; Inert atmosphere

3.1: boron trifluoride diethyl etherate / dichloromethane / 6 h / 175 °C / Sealed tube; Inert atmosphere; Schlenk technique

With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301187e

Reference yield:

: 576-22-7
2-Bromo-m-xylene

: 1415838-69-5
C₂₀H₂₃N₅O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere; Schlenk technique

1.2: 1 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: pyridinium chlorochromate / dichloromethane / 1 h / 25 °C / Inert atmosphere; Schlenk technique

3.1: copper(I) bromide / chloroform; ethyl acetate / 10 h / Inert atmosphere; Schlenk technique; Reflux

4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.08 h / 25 °C / Inert atmosphere; Schlenk technique

4.2: 2 h / 110 °C / Inert atmosphere; Schlenk technique

5.1: ethanol / 2 h / 175 °C / Sealed tube; Schlenk technique; Inert atmosphere

6.1: boron trifluoride diethyl etherate / dichloromethane / 6 h / 175 °C / Sealed tube; Inert atmosphere; Schlenk technique

With n-butyllithium; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; copper(I) bromide; In tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm301187e