3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

Base Information

Chemical Name:3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate
CAS No.:124244-06-0
Molecular Formula:C₂₃H₂₄O₂
Molecular Weight:332.442
Hs Code.:

Synonyms:

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Chemical Property of 3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

Chemical Property:

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Technology Process of 3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

There total 8 articles about 3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124244-05-9
3-(5,6-dihydro-2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

: 124244-06-0
3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 1h; Ambient temperature;
DOI:10.1021/jm00164a047

Reference yield:

: 27650-80-2
3-(2,4-dimethylphenyl)propan-1-ol

: 124244-06-0
3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

Guidance literature:: Multi-step reaction with 8 steps

1: 35.1 g / pyridine

2: 3.1 g / aluminum chloride / various solvent(s) / 2 h / Ambient temperature

3: 0.11 g / HCl (gas), Zn (activated) / diethyl ether / 1 h / 0 °C

4: oxalyl chloride / CH₂Cl₂ / 1.) room temperature, 30 min, 2.) reflux, 2 h

5: stannic chloride / CH₂Cl₂ / 0.5 h / Ambient temperature

6: 2.7 g / sodium borohydride / ethanol / 7 h / Ambient temperature

7: 1.6 g / phosphorus pentoxide / diethyl ether

8: 0.78 g / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / toluene / 1 h / Ambient temperature

With pyridine; hydrogenchloride; phosphorus pentaoxide; sodium tetrahydroborate; aluminium trichloride; oxalyl dichloride; tin(IV) chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc; In diethyl ether; ethanol; dichloromethane; toluene;
DOI:10.1021/jm00164a047

Reference yield:

: 124244-00-4
3-(2,4-dimethylphenyl)propyl benzoate

: 124244-06-0
3-(2,4,7-trimethylnaphthalen-1-yl)propyl benzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 3.1 g / aluminum chloride / various solvent(s) / 2 h / Ambient temperature

2: 0.11 g / HCl (gas), Zn (activated) / diethyl ether / 1 h / 0 °C

3: oxalyl chloride / CH₂Cl₂ / 1.) room temperature, 30 min, 2.) reflux, 2 h

4: stannic chloride / CH₂Cl₂ / 0.5 h / Ambient temperature

5: 2.7 g / sodium borohydride / ethanol / 7 h / Ambient temperature

6: 1.6 g / phosphorus pentoxide / diethyl ether

7: 0.78 g / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / toluene / 1 h / Ambient temperature

With hydrogenchloride; phosphorus pentaoxide; sodium tetrahydroborate; aluminium trichloride; oxalyl dichloride; tin(IV) chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc; In diethyl ether; ethanol; dichloromethane; toluene;
DOI:10.1021/jm00164a047