C₂₂H₂₈N₄O₆

Base Information

Chemical Name:C₂₂H₂₈N₄O₆
CAS No.:1428265-81-9
Molecular Formula:C₂₂H₂₈N₄O₆
Molecular Weight:444.488
Hs Code.:

C<sub>22</sub>H<sub>28</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₂H₂₈N₄O₆

Chemical Property:

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Technology Process of C₂₂H₂₈N₄O₆

There total 14 articles about C₂₂H₂₈N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₃₂N₄O₆

: 1428265-81-9
C₂₂H₂₈N₄O₆

Guidance literature:: With water; trifluoroacetic acid; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.01.070

Reference yield:

: 1428265-73-9
C₃₂H₃₇N₄O₉S^(1-)*Na⁽¹⁺⁾

: 1428265-81-9
C₂₂H₂₈N₄O₆

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: acetic acid; hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 48 h / 20 °C

3: trifluoroacetic acid; water / 24 h / 20 °C / Inert atmosphere

With sulfuric acid; palladium 10% on activated carbon; water; hydrogen; acetic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; water; ethyl acetate;
DOI:10.1016/j.bmc.2013.01.070

Reference yield:

: 14131-84-1
2,3:5,6-di-O-isopropylidene-α-D-mannofuranose

: 1428265-81-9
C₂₂H₂₈N₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran / 0.67 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: acetic acid / 3 h / Inert atmosphere; Reflux

3.1: thionyl chloride / tetrachloromethane / 0.5 h / Inert atmosphere; Reflux

3.2: 1 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: sulfuric acid / water; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: acetic acid; hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 48 h / 20 °C

7.1: trifluoroacetic acid; water / 24 h / 20 °C / Inert atmosphere

With thionyl chloride; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; sodium hydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; methanol; tetrachloromethane; water; ethyl acetate;
DOI:10.1016/j.bmc.2013.01.070