Technology Process of C26H24N2O4S
There total 12 articles about C26H24N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: sodium tetrahydroborate / methanol
2: 1H-imidazole
3: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II)
4: n-butyllithium / tetrahydrofuran
5: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
6: Burgess Reagent; triethylamine / acetonitrile / 80 °C
7: tetrabutyl ammonium fluoride / tetrahydrofuran
8: thionyl chloride / toluene
9: N-ethyl-N,N-diisopropylamine / acetonitrile
10: water; sodium hydroxide / ethanol
With
1H-imidazole; sodium tetrahydroborate; n-butyllithium; thionyl chloride; Burgess Reagent; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 7 steps
1: n-butyllithium / tetrahydrofuran
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / chloroform
3: Burgess Reagent; triethylamine / acetonitrile / 80 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran
5: thionyl chloride / toluene
6: N-ethyl-N,N-diisopropylamine / acetonitrile
7: water; sodium hydroxide / ethanol
With
n-butyllithium; thionyl chloride; Burgess Reagent; tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; ethanol; chloroform; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / toluene
2: N-ethyl-N,N-diisopropylamine / acetonitrile
3: water; sodium hydroxide / ethanol
With
thionyl chloride; water; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
ethanol; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.067