C₃₅H₃₀F₁₇NO₃S

Base Information

• Chemical Name: C₃₅H₃₀F₁₇NO₃S
• CAS No.: 1313585-77-1
• Molecular Formula: C₃₅H₃₀F₁₇NO₃S
• Molecular Weight: 867.667
• Mol file: 1313585-77-1.mol

Synonyms:

Chemical Property of C₃₅H₃₀F₁₇NO₃S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₃₀F₁₇NO₃S

There total 6 articles about C₃₅H₃₀F₁₇NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(bromomethyl)-4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzene → C35H30F17NO3S (1313585-77-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / -5 - 20 °C / Inert atmosphere; Darkness

2: caesium carbonate / acetonitrile / 3 h / 45 °C

3: ethanol; acetyl chloride / 16 h / 20 °C / Inert atmosphere

4: dichloromethane / 48 h / 20 °C

With ethanol; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride; In tetrahydrofuran; dichloromethane; acetonitrile; 4: Petasis reaction;

DOI:10.1016/j.tet.2011.05.039

Reference yield:

tert-butyl (4-methylbenzyl)(4-(2-perfluoroctylethyl)benzyloxy)carbamate (1313585-50-0) → C35H30F17NO3S (1313585-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; acetyl chloride / 16 h / 20 °C / Inert atmosphere

2: dichloromethane / 48 h / 20 °C

With ethanol; acetyl chloride; In dichloromethane; 2: Petasis reaction;

DOI:10.1016/j.tet.2011.05.039

Reference yield:

tert-butyl 4-(2-perfluoroctylethyl)benzyloxycarbamate (1313585-45-3) → C35H30F17NO3S (1313585-77-1)

Guidance literature:

Multi-step reaction with 3 steps

1: caesium carbonate / acetonitrile / 3 h / 45 °C

2: ethanol; acetyl chloride / 16 h / 20 °C / Inert atmosphere

3: dichloromethane / 48 h / 20 °C

With ethanol; caesium carbonate; acetyl chloride; In dichloromethane; acetonitrile; 3: Petasis reaction;

DOI:10.1016/j.tet.2011.05.039

upstream raw materials:

tert-butyl (4-methylbenzyl)(4-(2-perfluoroctylethyl)benzyloxy)carbamate

N-(4-methylbenzyl)-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

[4-(ethylsulfanyl)phenyl]boronic acid

2,2-dihydroxyacetic acid