2,2,7,7-tetraacetoxy-3,6-diphenyl-1-oxa-3,6-diazonia-4,5,8-triaza-2,7-diborata-1,2,7,8-tetrahydronaphthalene

Base Information

Chemical Name:2,2,7,7-tetraacetoxy-3,6-diphenyl-1-oxa-3,6-diazonia-4,5,8-triaza-2,7-diborata-1,2,7,8-tetrahydronaphthalene
CAS No.:111200-81-8
Molecular Formula:C₂₂H₂₃B₂N₅O₉
Molecular Weight:523.075
Hs Code.:

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Chemical Property of 2,2,7,7-tetraacetoxy-3,6-diphenyl-1-oxa-3,6-diazonia-4,5,8-triaza-2,7-diborata-1,2,7,8-tetrahydronaphthalene

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Technology Process of 2,2,7,7-tetraacetoxy-3,6-diphenyl-1-oxa-3,6-diazonia-4,5,8-triaza-2,7-diborata-1,2,7,8-tetrahydronaphthalene

There total 1 articles about 2,2,7,7-tetraacetoxy-3,6-diphenyl-1-oxa-3,6-diazonia-4,5,8-triaza-2,7-diborata-1,2,7,8-tetrahydronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.2%

: 69211-06-9
1,5-diphenylformazan-3-carboxamide

: 11113-50-1,14635-83-7
boric acid

: 111200-81-8
2,2,7,7-tetraacetoxy-3,6-diphenyl-1-oxa-3,6-diazonia-4,5,8-triaza-2,7-diborata-1,2,7,8-tetrahydronaphthalene

Guidance literature:: With acetic anhydride; In acetic anhydride; mixt. of H3BO3 and acetic anhydride is heated at 70-80°C until a clear soln. was obtained, addn. of acetic anhydride soln. of formazan, heated for 1.5h at 120°C; poured in cold water, dried in air, chromd. (silica gel, benzene-petroleum ether- ethyl acetate = 1:1:1), elem. anal.;