Technology Process of C31H35N3OS
There total 9 articles about C31H35N3OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol; chloroform;
at 0 ℃;
for 2h;
Inert atmosphere;
DOI:10.1039/c1ob06496g
- Guidance literature:
-
Multi-step reaction with 8 steps
1: hydrogenchloride / water; acetone / 0 h / 0 °C
2: sodium cyanide / ethanol / 0.5 h / 0 °C / Inert atmosphere
3: ammonia / ethanol / 24 h / 120 °C / Inert atmosphere; Saturated solution
4: pyridine / 12 h / 20 °C / Inert atmosphere
5: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
6: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
7: copper(II) sulfate / dichloromethane / 24 h / 20 °C / Inert atmosphere
8: sodium tetrahydroborate / methanol; chloroform / 2 h / 0 °C / Inert atmosphere
With
pyridine; hydrogenchloride; sodium cyanide; sodium tetrahydroborate; tetrabutyl ammonium fluoride; ammonia; Dess-Martin periodane; copper(II) sulfate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; acetone;
DOI:10.1039/c1ob06496g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 12 h / 20 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
3: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere
4: copper(II) sulfate / dichloromethane / 24 h / 20 °C / Inert atmosphere
5: sodium tetrahydroborate / methanol; chloroform / 2 h / 0 °C / Inert atmosphere
With
pyridine; sodium tetrahydroborate; tetrabutyl ammonium fluoride; Dess-Martin periodane; copper(II) sulfate;
In
tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1039/c1ob06496g