C₁₁H₁₄N₂O₂

Base Information

• Chemical Name: C₁₁H₁₄N₂O₂
• CAS No.: 1452161-84-0
• Molecular Formula: C₁₁H₁₄N₂O₂
• Molecular Weight: 206.244
• Mol file: 1452161-84-0.mol

Synonyms:

Chemical Property of C₁₁H₁₄N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₄N₂O₂

There total 6 articles about C₁₁H₁₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H12N4O2 (1452161-83-9) → C11H14N2O2 (1452161-84-0)

Guidance literature:

With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 2h; Cooling with ice;

DOI:10.1039/c3cc43257b

Reference yield:

C11H12BrNO2 (1452161-82-8) → C11H14N2O2 (1452161-84-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / water; acetone / 4 h / 20 °C / Cooling with ice

2: triphenylphosphine; water / tetrahydrofuran / 2 h / 20 °C / Cooling with ice

With sodium azide; water; triphenylphosphine; In tetrahydrofuran; water; acetone;

DOI:10.1039/c3cc43257b

Reference yield:

2-nitrocinnamaldehyde (1466-88-2,66894-06-2) → C11H14N2O2 (1452161-84-0)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium tetrahydroborate / methanol / 0.5 h / 20 °C / Cooling with ice

2: ammonium hydroxide; iron(II) sulfate heptahydrate / methanol; water / 4 h / 80 °C

3: sodium hydrogencarbonate / acetone / 2 h / Cooling with ice

4: phosphorus tribromide / diethyl ether / 0.5 h / 20 °C / Cooling with ice

5: sodium azide / water; acetone / 4 h / 20 °C / Cooling with ice

6: triphenylphosphine; water / tetrahydrofuran / 2 h / 20 °C / Cooling with ice

With ammonium hydroxide; sodium tetrahydroborate; sodium azide; iron(II) sulfate heptahydrate; water; phosphorus tribromide; sodium hydrogencarbonate; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; water; acetone;

DOI:10.1039/c3cc43257b

upstream raw materials:

C₁₁H₁₂BrNO₂

C₁₁H₁₂N₄O₂

3-(2-nitrophenyl)prop-2-en-1-ol

2-nitrocinnamaldehyde

Downstream raw materials:

(E)-N-methoxycarbonyl-3-(2-methoxycarbonylaminophenyl)-2-propeneamine