C₂₈H₃₈N₄O₇

Base Information

• Chemical Name: C₂₈H₃₈N₄O₇
• CAS No.: 1310328-66-5
• Molecular Formula: C₂₈H₃₈N₄O₇
• Molecular Weight: 542.632
• Mol file: 1310328-66-5.mol

Synonyms:

Chemical Property of C₂₈H₃₈N₄O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₃₈N₄O₇

There total 6 articles about C₂₈H₃₈N₄O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(9S,12S)-methyl 12-benzyl-16,16-dimethyl-3,11,14-trioxo-1-phenyl-2,15-dioxa-4,10,13-triazaheptadecane-9-carboxylate (68802-90-4) → C28H38N4O7 (1310328-66-5)

Guidance literature:

With hydroxylamine potassium salt; In methanol; at 25 ℃; for 12h;

DOI:10.1016/j.bmc.2011.03.028

Reference yield:

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) → C28H38N4O7 (1310328-66-5)

Guidance literature:

Multi-step reaction with 2 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 5 h / 25 °C

2: hydroxylamine potassium salt / methanol / 12 h / 25 °C

With hydroxylamine potassium salt; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In methanol; dichloromethane;

DOI:10.1016/j.bmc.2011.03.028

Reference yield:

N6-[(benzyloxy)carbonyl]-L-lysine (1155-64-2,57705-97-2,67178-46-5,25931-47-9) → C28H38N4O7 (1310328-66-5)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride / 6 h / 25 °C

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / dichloromethane / 5 h / 25 °C

3: hydroxylamine potassium salt / methanol / 12 h / 25 °C

With hydrogenchloride; hydroxylamine potassium salt; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In methanol; dichloromethane;

DOI:10.1016/j.bmc.2011.03.028

upstream raw materials:

L-lysine

(9S,12S)-methyl 12-benzyl-16,16-dimethyl-3,11,14-trioxo-1-phenyl-2,15-dioxa-4,10,13-triazaheptadecane-9-carboxylate

N-tert-butoxycarbonyl-L-phenylalanine

N₆-[(benzyloxy)carbonyl]-L-lysine