N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide

Base Information

• Chemical Name: N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide
• CAS No.: 117124-94-4
• Molecular Formula: C₁₉H₁₄Cl₂N₂O
• Molecular Weight: 357.239
• Mol file: 117124-94-4.mol

Synonyms:

Chemical Property of N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide

There total 1 articles about N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-2,6-dichlorophenol (5930-28-9) + N-phenyl-benzimidoyl chloride (4903-36-0) → N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide (117124-94-4)

Guidance literature:

With triethylamine; In acetonitrile; at 10 ℃; for 2h;

Reference yield:

N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide (117124-94-4) → 2,6-dichloro-4-(N-phenylbenzenecarboximidoyl)imino-2,5-cyclohexadien-1-one (117125-02-7)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; at 23 - 25 ℃; for 0.5h;

Reference yield:

N-(3,5-dichloro-4-hydroxyphenyl)-N'-phenylbenzenecarboximidamide (117124-94-4) → 5,7-dichloro-1,2-diphenyl-6-hydroxybenzimidazole (117125-11-8)

Guidance literature:

Multi-step reaction with 2 steps

1: active MnO₂ / CH₂Cl₂ / 0.5 h / 23 - 25 °C

2: 35 percent / acetic acid / 0.17 h / 50 °C

With manganese(IV) oxide; acetic acid; In dichloromethane;

upstream raw materials:

4-amino-2,6-dichlorophenol

N-phenyl-benzimidoyl chloride

Downstream raw materials:

2,6-dichloro-4-(N-phenylbenzenecarboximidoyl)imino-2,5-cyclohexadien-1-one

5,7-dichloro-1,2-diphenyl-6-hydroxybenzimidazole

Refernces