6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine

Base Information

Chemical Name:6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine
CAS No.:132652-98-3
Molecular Formula:C₁₉H₁₄BrNS
Molecular Weight:368.297
Hs Code.:

6-(4-bromobenzyl)-6H-dibenzo<c,e><1,2>thiazine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine

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Technology Process of 6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine

There total 4 articles about 6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-(4-bromobenzyl)-6H-dibenzo<1,2>thiazin-5-ium perchlorate

: 132652-98-3
6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine

Guidance literature:: With sodium hydroxide; In dichloromethane; at 0 ℃; Yield given;
DOI:10.1016/S0040-4039(00)97232-0

Reference yield:

: 132652-82-5
2'-(4-Bromo-benzylsulfanyl)-biphenyl-2-ylamine

: 132652-98-3
6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine

Guidance literature:: With sodium hydroxide; tert-butylhypochlorite; Yield given. Multistep reaction; 1) CH₂Cl₂, -70 to -65 deg C to r.t., overnight;

Reference yield:

: 35883-85-3
2-amino-2'-nitrobiphenyl hydrochloride

: 132652-98-3
6-(4-bromobenzyl)-6H-dibenzo<1,2>thiazine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaNO₂, aq.HCl / 1) 0-5 deg C, 2 h, 2) H₂O, CH₂Cl₂, overnight

2: 1) LiAlH₄ / 1) THF, 2 h, 2) EtOH, reflux, 1 h

3: 1) t-BuOCl, 2) aq.NaOH / 1) CH₂Cl₂, -70 to -65 deg C to r.t., overnight

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; tert-butylhypochlorite; sodium nitrite;