O,N-Diacetylpseudosolasodine

Base Information

• Chemical Name: O,N-Diacetylpseudosolasodine
• CAS No.: 1181-89-1
• Molecular Formula: C₃₁H₄₇NO₄
• Molecular Weight: 497.718
• Mol file: 1181-89-1.mol

Synonyms:

Chemical Property of O,N-Diacetylpseudosolasodine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O,N-Diacetylpseudosolasodine

There total 7 articles about O,N-Diacetylpseudosolasodine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3β-Acetoxy-26-acetylamino-16,22-secofurost-5-ene-16,22-dione (63342-06-3,76193-70-9) → O,N-Diacetylpseudosolasodine (1181-89-1,5672-30-0,50895-40-4)

Guidance literature:

With hydrogen; acetic acid; nickel; Yield given; 1.) ethanol, 50 deg C, 50 atm, 2 h, 2.) 20 min;

DOI:10.1007/BF00763417

Reference yield:

→ 3β-Acetoxy-27-acetamino-25α-5,20(22)-furostadien (1181-89-1,5672-30-0,50895-40-4)

Guidance literature:

3β-Hydroxy-27-amino-25α-5,20(22)-furostadien, Acetanhydrid, Py. (25grad, 18 Std.);

DOI:10.1021/ja01467a045

Reference yield:

→ Pseudosolasodin-diacetat (1181-89-1,5672-30-0,50895-40-4)

Guidance literature:

1) Solasodin-diacetat, HCl (CH2Cl2, 20 min, Raumtemp.);

DOI:10.1021/jo01075a029

upstream raw materials:

3β-Acetoxy-26-acetylamino-16,22-secofurost-5-ene-16,22-dione