C₂₂H₃₄O₄Si

Base Information

Chemical Name:C₂₂H₃₄O₄Si
CAS No.:1373885-37-0
Molecular Formula:C₂₂H₃₄O₄Si
Molecular Weight:390.595
Hs Code.:

C<sub>22</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₄O₄Si

Chemical Property:

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Technology Process of C₂₂H₃₄O₄Si

There total 7 articles about C₂₂H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1373885-36-9
C₁₇H₂₄O₄

: 1066-54-2
trimethylsilylacetylene

: 1373885-37-0
C₂₂H₃₄O₄Si

Guidance literature:: With zinc trifluoromethanesulfonate; triethylamine; In toluene; at 20 - 60 ℃; for 48h; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: 1373885-33-6
C₁₆H₂₄O₄

: 1373885-37-0
C₂₂H₃₄O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: 1H-imidazole; iodine; triphenylphosphine / toluene / 20 h / 20 °C

2: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 4 h / -40 - 20 °C

3: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 72 h / 20 °C

4: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

5: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium periodate; copper(l) iodide; osmium(VIII) oxide; water; iodine; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; water; acetone; toluene; 5: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090

Reference yield:

: 1373885-32-5
C₁₈H₂₆O₅

: 1373885-37-0
C₂₂H₃₄O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2: 1H-imidazole; iodine; triphenylphosphine / toluene / 20 h / 20 °C

3: N,N,N,N,N,N-hexamethylphosphoric triamide; copper(l) iodide / tetrahydrofuran / 4 h / -40 - 20 °C

4: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 72 h / 20 °C

5: sodium periodate / tetrahydrofuran; water / 0.5 h / 0 - 20 °C

6: zinc trifluoromethanesulfonate; triethylamine / toluene / 48 h / 20 - 60 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium periodate; copper(l) iodide; osmium(VIII) oxide; lithium aluminium tetrahydride; water; iodine; zinc trifluoromethanesulfonate; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; water; acetone; toluene; 6: Carreira's addition;
DOI:10.1016/j.tetlet.2012.02.090