tricyclo<3.3.1.1^3,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate

Base Information

• Chemical Name: tricyclo<3.3.1.1^3,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate
• CAS No.: 139657-37-7
• Molecular Formula: C₃₂H₃₈N₂O₂
• Molecular Weight: 482.666

Synonyms:

Chemical Property of tricyclo<3.3.1.1^3,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate

Chemical Property:

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Useful:

Technology Process of tricyclo<3.3.1.1^3,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate

There total 5 articles about tricyclo<3.3.1.1^3,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromo-3-phenylpropane (637-59-2) → tricyclo<3.3.1.13,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate (139657-37-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 65 percent / 110 °C

2: sodium hydride / toluene / 0.33 h / Heating

3: toluene / 1 h / Heating

With sodium hydride; In toluene;

DOI:10.1021/jm00086a017

Reference yield:

bromotriphenyl(3-phenylpropyl)-λ5-phosphane (5717-39-5) → tricyclo<3.3.1.13,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate (139657-37-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / toluene / 0.33 h / Heating

2: toluene / 1 h / Heating

With sodium hydride; In toluene;

DOI:10.1021/jm00086a017

Reference yield:

N-[(2-adamantyloxy) carbonyl]-α-methyl-D-tryptophan methyl ester (130406-39-2) → tricyclo<3.3.1.13,7>dec-2-yl -<1-(1H-indol-3-ylmethyl)-1-methyl-5-phenyl-2-pentenyl>carbamate (139657-37-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 91 percent / lithium aluminum hydride / tetrahydrofuran; diethyl ether / 0.33 h / 0 °C

2: 67 percent / N-methylmorpholine N-oxide, molecular sieves (4A), tetra-n-propylammoniumperruthenate (TPAP) / CH₂Cl₂ / 0.5 h / Ambient temperature

3: toluene / 1 h / Heating

With lithium aluminium tetrahydride; tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;

DOI:10.1021/jm00086a017

upstream raw materials:

(triphenylphosphonio)-3-phenyl-1-propanide

tricyclo<3.3.1.1^3,7>dec-2-yl (R)-<1-formyl-2-(1H-indol-3-ylmethyl)-1-methylethyl>carbamate

1-Bromo-3-phenylpropane

bromotriphenyl(3-phenylpropyl)-λ⁵-phosphane

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