Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate

Base Information

Chemical Name:Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate
CAS No.:135523-98-7
Molecular Formula:C₂₂H₂₄N₂O₇
Molecular Weight:428.442
Hs Code.:

Benzyl (2S,4R,1'S)-2-(tert-butyl)-4-<hydroxy-(4-nitrophenyl)methyl>-5-oxo-3-oxazolidinecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate

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Technology Process of Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate

There total 1 articles about Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 119323-02-3
(+)-2-(tert-Butyl)-5-oxooxazolidin-3-carbonsaeure-bezylester

: 135523-98-7
Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate

Guidance literature:: With lithium hexamethyldisilazane; Yield given. Multistep reaction; 1) THF, -78 deg C, 15-20 min, 2) THF, -100 deg C, 15-20 min;

Reference yield:

: 135523-98-7
Benzyl (2S,4R,1'S)-2-(tert-butyl)-4--5-oxo-3-oxazolidinecarboxylate

: 123410-35-5
(-)-(2R,3S)-N-(Dichloroacetyl)-3-(4-nitrophenyl)serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1,4-cyclohexadiene, 2) H₂O / 1) 10percent Pd/C / 1) EtOH, THF, 20 deg C, 20 min, 2) 5 min

2: 1) 1 N aq.NaOH / 1) 1,4-dioxane, r.t., 12 h, 2) MeOH, Et₂O, 45 min

With sodium hydroxide; cyclohexa-1,4-diene; water; palladium on activated charcoal;