K[Al(OC(CF₃)2Ph)4]

Base Information

Chemical Name:K[Al(OC(CF₃)2Ph)4]
CAS No.:1253641-83-6
Molecular Formula:C₃₆H₂₀AlF₂₄O₄*K
Molecular Weight:1038.59
Hs Code.:

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Chemical Property of K[Al(OC(CF₃)2Ph)4]

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Technology Process of K[Al(OC(CF₃)2Ph)4]

There total 1 articles about K[Al(OC(CF₃)2Ph)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 16853-85-3
lithium aluminium tetrahydride

: 718-64-9
1,1,1,3,3,3-hexafluoro-2-phenylisopropyl alcohol

: potassium chloride

: 1253641-83-6
K[Al(OC(CF₃)2Ph)4]

Guidance literature:: In water; toluene; (Ar), Schlenk techniques; slurrying LiAlH4 in toluene, addn. of F compd.at room temp., heating under reflux for 3 h, evapn. in vacuo, dissolvin g in Et2O, treatment with satd. aq. KCl, stirring 3 h at room temp.; layer separation, pptn., washing with satd. aq. KCl, drying (MgSO4), filtration, evapn. in vacuo, dissolving in CH2Cl2, layering with n-pentane at 0°C, isolation of crystals, elem. anal.;
DOI:10.1039/c1dt10280j

Reference yield: 90.0%

: 1253641-83-6
K[Al(OC(CF₃)2Ph)4]

: silver nitrate

: 75-05-8,26809-02-9
acetonitrile

: [Ag(acetonitrile)2][Al(OC(CF₃)2Ph)4]

Guidance literature:: In acetonitrile; (Ar), Schlenk techniques; in dark addn. of soln. of AgNO3 in MeCN to soln. of Al complex in MeCN, stirring for 15 min; addn. of Et2O, stirring for 15 min, evapn. in vacuo, dissolving in CH2Cl2, filtration, evapn. in dark, elem. anal.;
DOI:10.1039/c1dt10280j