Technology Process of C2HF3O2*C40H37Br2N10O2P
There total 5 articles about C2HF3O2*C40H37Br2N10O2P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 5 h / 40 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: trifluoroacetic acid / dimethyl sulfoxide / 5 h / 40 °C
3.1: trifluoroacetic acid / dichloromethane / 23 °C / Inert atmosphere
4.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 3 h / 23 °C / Inert atmosphere
4.2: 6 h / 50 °C / Inert atmosphere
5.1: water / preparative HPLC; Inert atmosphere
With
calcium borohydride bis(tetrahydrofuran); trifluoroacetic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1021/ja207386q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 3 h / 23 °C / Inert atmosphere
1.2: 6 h / 50 °C / Inert atmosphere
2.1: water / preparative HPLC; Inert atmosphere
With
calcium borohydride bis(tetrahydrofuran);
In
tetrahydrofuran; water;
DOI:10.1021/ja207386q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 23 °C / Inert atmosphere
2.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 3 h / 23 °C / Inert atmosphere
2.2: 6 h / 50 °C / Inert atmosphere
3.1: water / preparative HPLC; Inert atmosphere
With
calcium borohydride bis(tetrahydrofuran); trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ja207386q
